GCMS DFTPP calibration report, Feb 5 2002

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Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02”

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NYC 9/11 Public Portal Document

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Data File : C:\MSDCHEM\1\5973N\02FEB05\0201B.D Vial: 1 Acq On : 5 Feb 2002 10:42 am Operator: Sample : lab blank 2/1 Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l..-\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

5.92 0.27 ug/L 180036 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

13-(CYCLOHEX-3’ -EN-YL)PROPANOL $$.. . 174 C8H1404 015745-87-6 40 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 40 3 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 4 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 9 Abundance Scan 223 (5.920 min): 0201 B.D (-) m/z 73.10 100.00% 73

5000 43 57 5.60 5.80 6.00 6.20 ' ' O—PP] - 11 ‘" 11'' 'I' 11 । 87 103 '11 r 1 i'1" r'' " i1' " i' " 111" ' i " " i11111" " I " " 11 m/z 43.10 23.31% mfz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 -A ’I । । । । । 5.60 5.80 6.00 6.20 43 m/ z 41.10 9.41% 27 87 0- TT ■ i"55" i1" ' , ii ' Hi " ■ ■ i " " 113 174 i '111 ■ " I " " r " 1111" I " ITT' " 11'1 miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 1l1 '-r 1 1 1 1 1 ■ ■ i ■ ■ ■ ■ । 5.60 5.80 6.00 6.20 5000 m/ Z 45.10 9.28% 43 27 55 87 113 174 T1 HP . i o1TTTTgT 1111111' II I 'I ■'1' I TCIOuanndn n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... .......A....... I, ............... 30 5.60 5.80 6.00 6.20 73 m/z 71.10 5.96%

5000 44 58 15 — o i I'' " I 'r ■ " i'11 •' i " 1' I " 1' I " ■' i" 11 r 1 ‘' i " " I " 111" " I " " 11" 111 ' 1 i ■ 1 ‘ 1 i ■ ■ ■ • i ‘ 1 1 1 1 1 ' 1 1 I n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5,60 5.80 6.00 6.20

0201B.D SCAN508.M Thu Feb 21 10:18:57 2002 Page 5

NYC-WTC_000004788

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NYC-WTC_000004788Source: NYC Law Department, mirrored locally

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