GCMS blank analysis results for sample AE03508, March 2002

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Library Search Compound Report

* Data File : C:\MSDCHEM\l\5973N\02MAR08\0219B.D Vial: 1 Acq On : 8 Mar 2002 10:39 am Operator: Sample : lab blank 2/19 Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1. . .\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.89 4.25 ug/L 2086540 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-(CYCLOHEX-3’ -EN-YL)PROPANOL $$... 174 C8H1404 015745-87-6 33 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 3 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H140 000994-05-8 33 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 223 (5.891 min): 0219B.D (-) m/z 73.10 100.00% 73

5000 43 ' 1 I ' 1 ' 1TT 87 103 _ , 5.60 5.80 6.00 6.20 I 1 55 ,i , m/z 43.10 25.31% 0-'l | I I K | I ll > TTTT I TTTTTT I T ITTTmnt miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3‘-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 1-1-1 r1 111T 5.60 5.80 6.00 6.20 43 m/z 45.10 9.56% 27 ..... 0- pt ■ i ■ ■ ■ J , 87 11 •" •!* 111111 TT . i, > ।.... । 113 ।..., ।... > ।. 11... ।।. 1111. ।. 174 miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1 ,3]dioxolan-2-ylpropyl ester 73 ......... ***1/1/1/1/11/1/. f-r-i-i-r- 5.60 5.80 6.00 6.20 5000 m/z 41.10 9.11%

miz—> 27 43

0- ■ i ■1 “ I ■ TTHTTT ,' " 11'87 Abundance 55 । 113 111 “ “ i “ “ i 174 “ i1 “ ‘ i “ “ i' ■ ■ ■ i “ ‘ • i11 ■' i11' ■ t ■ 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 #9702: Butane, 2-methoxy-2-methyl- $$ Ether, methyl tert-p... 73 TAI

m/z 5.60 1 n —PPM T nnuur 5.80 6.00 6.20 71.00 6.61%

miz—> 5000

27 45 55

O-pp4 ■ 1 — - l ■ • । • ■ ■ 11 • ■ > > । 2030405060 70 87

‘ । “1 ■ i “ “ i “ “ i1 “11 ■ 8090 100 110 120 130 140 150 160 170 180 i' ■ ■ ■ i “ “ i1 5.60 1 5.80 6.00 6.20

0219B.D HP022102.M Fri Mar 15 10:08:43 2002 Page 8

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