GCMS blank analysis results for sample AE03508, March 2002

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Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02MAR08\0219B.D Vial: 1 Acq On : 8 Mar 2002 10:39 am Operator: Sample : lab blank 2/19 Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 Oxirane, butyl- (CAS) $$ 1,... Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

5.02 0.09 ug/L 45637 1,4-Dichlorobenzene~d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Oxirane, butyl- (CAS) $$ 1,2-Epo... 100 C6H120 001436-34-6 38 2 3-hydroxy-4,4-dimethyl .gamma. B... 130 C6H10O3 052126-90-6 37 3 Oxirane, propyl- 86 C5H10O 001003-14-1 33 4 Oxirane, propyl- (CAS) $$ Propyl... 86 C5H10O 001003-14-1 33 Abundance Scan 146 (5.022 min): 0219B.D (-) m/z 71.00 100.00% 43 71

5000

51 59

85 \ AA... 4.60 4.80 5.00 5.20 5.40

miz-> IHL... . 0 n-[ 1 1 1 I । r: I T I "IIEI’TTTI 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 1111 > 111111.... ।.... ।.... ।.... ।.. m/z 43.00 90.97% Abundance " #8516: Oxirane, butyl- (CAS) $$ 1,2-Epoxyhexane $$ Butylox... 41 71

5000 56 M4.80A5.00AAAA 4.60 5.20 5.40 m/z 41.10 79.64% 27 RS Of _ _ _ . _ 11 ,1 85... 100.. miz-> 2 25 3035 40 45"50556o 657 7580 85’9095/100105 Abundance #26149: 3-hydroxy-4,4-dimethyl .gamma. Butanolactone $$ Pa... 43 7 Anal 4.60 4.80 5.00 5.20 5.40 5000 m/z 69.10 42.85% 57 31 0 - +—7 H -rp1’11’117!m1’1TTT II’ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #4132: Oxirane, propyl- ■ ■ i ■ ■ > . i • * 41 4.60 4.80 5.00 5.20 5.40 71 m/z 59.00 37.85%

5000

56

4+14 0 rgrrnjiT. ’U9l’2111111 , 85 TTI—urmmm1umut———"ET—’"T -AAA A miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 4.60 4.80 5.00 5.20 5.40

0219B.D HP022102.M Fri Mar 15 10:08:43 2002 Page 7

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