DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004935–000005145

Folder label: “GCMS X 2/1/02 A 2/27/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB27\0201B.D Vial : 1 Acq On : 27 Feb 2002 10:33 am Operator: Sample : lab blank 2/1 Inst : Instrumen Mise : February 27, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 5 3 -(CYCLOHEX-3'-EN-YL)PROPAN. .. Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 5.94 0.44 ug/L 198695 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

13-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 36 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 36 3 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 4 1,3-Dioxolane, 2-heptyl-___________ 172 C10H20O2 004359-57-3 9 Abundance Scan 227 (5.936 min): 0201 B.D (-) m/ z 73.10 100.00% 73

5000 43 5.60 5.80 6.00 6.20 , 87 103 0 .. ।'... ।.... ।. .. 11,17755... 1 110] m/z 43.10 25.01%

.. 1... m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 --nddd*ndn/dd/n/1//7//"/"R 5.60 5.80 6.00 6.20 43 m/z 45.00 10.28% 27 55 , | ,1 " i111 87' i1" ' i " ■ ■ 113 174 0 P 114 i ‘ i " ■ ■ i ■ " ■ i " 1' i1" 11 ■ ■1' i1'111 ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 7)3 1 1 । 1 ■ ■ ■ । 5.60 5.80 6.20 5000 m/z 41.10 7.25%

43 27 55 . , 87 113 174 0--TT Tp m/z-> Abundance 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... 30 ‘ । l > । 5.60 h..... ' i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i 5.80 6.00 6.20 73 m/z 71.10 5.10%

5000- 44 58 y 15 - 0 11 r 1 11 — TTTTTTTTTLTTTTTTUTLTTTTTTTTTLTTTTITTTTIUTTTIUTTTTTTTWTTTT ‘I‘‘ ‘I’* m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

201B.D HP022102.M Thu Feb 28 08:46:40 2002 Page 7

NYC-WTC_000004955

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NYC-WTC_000004955Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999