GCMS DFTPP calibration report, Feb 5 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02FEB05\0201B .D Vial: 1 Acq On : 5 Feb 2002 10:42 am Operator: Sample : lab blank 2/1 Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP020702 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 2,2-Dimethoxybutane Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 4.24 0.40 ug/L 261555 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2,2-Dimethoxybutane 118 C6H14O2 003453-99-4 74 2 Glycine, methyl ester $$ NH2CH2C... 89 C3H7NO2 000616-34-2 38 3 Ethane, isothiocyanate- $$ Isoth... 87 C3H5NS 000542-85-8 9 4 2-Propenenitrile, 2-chloro- $$ A... 87 C3H2C1N 000920-37-6 9 Abundance Scan 76 (4.241 min): 0201 B.D (-) m/z 87.10 100.00% 87

55 5000 43

A ■p ’ 1T I 1 1 ■' 1 1 1 1 1 1 1 1 r 1 103 3.80 4.00 4.20 4.40 4.60 O+ 149 . TITT —mmmmP H l . 4 71 m/z 89.10 88.88% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #17888: 2,2-Dimethoxybutane 55 87

5000 ... 11... 3.80 4.00 4.20 4.40 4.60 40 45 27 m/z 55.10 56.09% 33 I 92 103 0 "r"‘i‘ IT+pannsenunalusyann " i' " ‘ i" " r " ■ i" —mmT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 Abundance #5025: Glycine, methyl ester $$ NH2CH2COOCH3 89 A 11 3.80 4.00 4.20 4.40 4.60 5000 m/ Z 43.10 47.13% 44 , 59 I 54 66 i ■1 >■।11■■ 1111 TPm 0 ’’’1 l""i TTT n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #4317: Ethane, isothiocyanato- $$ Isothiocyanic acid, ethy... 87 3.80 4.00 4.20 4.40 4.60 59 m/z 45.10 14.61%

5000 27 72

0- 34 46 I".. .. ....... 111' ■ ■ -1 • • ■11 ■ ■" I" ■ ■ l • ■ • .0. ... m/z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 3.80 4.00 4.20 4.40 4.60

0201B.D SCAN508.M Thu Feb 21 10:18:57 2002 Page 4

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