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GC/MS analysis results for sample AD23082, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD23082 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087875–000087892

Folder label: “GC/MS Scan 9/21/01

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NYC 9/11 Public Portal Document XJJ-J. jr L_»<_4.J_ X1 U

■Data File : C:\HPCHEM\1\DATA\OCT0401\23082.D Vial: 2 Acq On : 4 Oct 2001 4:30 pm , Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Butyl hexadecanoate Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

29.53 0.84 ug/1 119861 Chrysene-dl2 33.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butyl hexa^canoate 312 C20H40O2 000000-00-0 64 2 2-Decene/9-methyl-, (Z)- 154 C11H22 074630-24-3 25 3 Cyclobu-cane, 1-hexyl-2,3-dimethyl- 168 C12H24 055170-84-8 25 4 Cycloctane, 1,1-dimethyl-2-octyl- 196 C14H28 062338-30-1 25 Abundance Scan 2667 (2‘9:526 min): 2308276 0 m/F '56.00 100.00% 5S

5000 43 73 129 257

m/2-> 20 40 IM 60 .M. JJ I 143157171 185 I T , . 1 I , . • T, I I , . I . • . 80 I, ,11. I, , 100 120 140..160 180 200 220 240 260 280 300 2^ | , I ,, . ,, I I I 312 p-TT-rp-r-f-p- 29.20 29.40 29.60 29.80 m/z 57.0 44.13% ^Abundance #44549: Butyl iiexadecanoate 50

5000 258 i 29.20 29.40 29.60 29.80

m/z-> 'Abundance 20 40 u 60 73

80 I , I, I .1' ' Vp-T-W-p-TT-T 157171 100 120 140 160 180 200 220 240 260 280 300 #11056:2-Decene. 9-mett,yl-. (Z)- 214 } ' ’ ' ' I 240 I 312 m/z 43.05 37.62%

56 I 69 4^ 29.20 29.40 29.60 29.80 m/z 41.05 36.57% 27 42 'i 83

I I • m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #14719: Cyclobutane, 1-hexyl-2.3-dimethyl- 29.20 29.40 29.60 29.80 m/z 73.00 29.33% 5000

70

Ti/z-> 20 42 I 40 I 80X 100 120 140.160 60 . .180,,,, 200 220 240 260 280... 300 ........... i........... 29.20 29.40 29.60 29.80

23082.D NP091101.M Tue Oct 09 12:23:39 2001 Page 3

NYC-WTC_000087884

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NYC-WTC_000087884Source: NYC Law Department, mirrored locally

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