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GC/MS analysis results for sample AD22978, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22978 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087754–000087772

Folder label: “GC/MS Scan 9/21/01

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NYC 9/11 Public Portal Document

' Data File C:\HPCHEM\1\DATA\OCT03 01\22978 . D Vial: 4 Acq On 3 Oct 2001 3:35 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Butyl hexadecanoate Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

29.53 0.56 ug/1 78996 Chrysene-dl2 33.15

Hit# of 5 intative ID MW MolForm CAS# Qual

1 Butyl hex. ecanoate 312 C20H40O2: 000000-00-0 37 2 Oxirane, > ,3-bis(1-methylethyl)t 128 C8H16O 054644-32-5 37 3 1-Hexen^ 2-methyl- 98 C7H14 006094-02-6 27 4 1,3-HeXanediol, 2-ethyl- 146 C8H18O2 000094-96-2 25 /Abundance Scan 2667 (29.528 min): 22978.D (-) m/z 56.00 100.00% 5)6

5000 41 73 129 257 I 14315717085 213 ^39 J 29.20 29.40 29.60 29.80 JJ p^T-iYTT-HYTTH-TyvTTppTT-rp-iS-TTp-TTHy-TTnr^^ p-T-rp-T-i-rry 312 m/z 57.00 , 44.02% m/z~> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #44549: Butyl hexadecanoate 5(6

5000 258 29.20 29.40 29.60 29.80 A. 73 240 312 116129 m/z 41.0,5 38.01%

m/z-> 20 40 (1 60 80 15717085 Vp-rVryT-rTTyTT-Tp-TT-Vp-^ 214 I' ' ' ' I 100 120 140 160 180 200 220 240 260 280 300 I ' ' ' ’ I

Abundance #5067: Oxirane, 2,3-bis(1-methylethyl)-, trans- 5^ 41 ; 29.20 29.40 29.60 29.80 KJsEE m/z 34.55%

m/z--> /Abundance 20 . . jX40 60 80 113 128 p-TTn-j-rTT-ry-TT-rry ■p-r-r-ry I ' ' ' ' I 100 120 140 160 180 200 220 240 260 280 300 #1354:1-Hexene, 2-methyl- IA [AA yp \ 5(6 29.20 29.40 29.60 29.80 m/z 55.00 28.96% 41 5000 27 i.i , 83 rr I I I . . p-. . . I pr-r-r-rp-n-ry I ' ‘ ' I T I I .1 I I J I I Ti/z~> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80

22978.D NP091101.M Tue Oct 09 09:51:20 2001 Page 3

NYC-WTC_000087763

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