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GC/MS analysis results for sample AD23125, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD23125 conducted on October 12, 2001.

NYC-WTC_000088023–000088043

Folder label: “GC/MS Scan 9/24/01

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NYC 9/11 Public Portal Document

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Data File C:\HPCHEM\1\DATA\OCT0401\23125 .D Vial: 13 Acq On 5 Oct 2001 3:16 am Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise -Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★it***** Peak Number 3 Butyl hexadecanoate Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

29.53 2.13 ug/1 420338 Chrysene-dl2 33.16

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butyl hpi< :adecanoate 312 C20H40O2 000000-00-0 59 2 1-Hex^f^, 2-methyl- 98 C7H14 006094-02-6 27 3 Oxirane, 2,3-bis(1-methylethyl)t 128 C8H16O 054644-32-5 23 4 1^-Hexanediol, 2-ethyl- 146 C8H18O2 000094-96-2 23 ^XbundSnee Scan 2668 (29.533 min): 23125.D (-) m/ z 56.00 100.00% 55

5000 41 73 257 ' 'I JL LlLOXill3l5z^^ 239 XX 312 -r+n 29.20 29.40 29.60 29.80 m/z 57.00 46.04% ■n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #44549: Butyl hexadecanoate

5000 258 29.20 29.40 29.60 29.80 73 240 312 129 m/z 41.05 37.26% J I 1571711^ 214 Mz-> 20 40 60 100 120 140 160 180 200 220 240 260 280 300 ^kbundance #63261; 1-Hexene, 2-metliyl- 56 ' ' I ' ' 29.20 29.40 29.60 29.80 41 SsH m/z 43.00 36.10% 27 70 98 n/z-> Abundance 20 40

41 60 55 80 100 120 140 160 180 200 220 240 260 280 300 #5067; Oxirane, 2.3-bis(1-methyiethyl)-, trans- r' ' iVU. 29.20 29.40 29.60 29.80 m/ Z 73.00 30.26% 5000 73

m/z-> 20 40 A 60 113128 80 100 120 140 160 180 200 220 240 260 .280 300 I ' ' ' ' .1 ' ' ' ' I 29.20 29.40 29.60 29.80

23125.D NP091101.M Tue Oct 09 12:43:18 2001 Page 3

NYC-WTC_000088032

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