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GC/MS analysis results for sample AD23082, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD23082 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087875–000087892

Folder label: “GC/MS Scan 9/21/01

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Scanned page image, NYC-WTC_000087883
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NYC 9/11 Public Portal Document

•Data File C:\HPCHEM\1\DATA\OCT0401\23082.D Vial: 2 Acq On 4 Oct 2001 4:30 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L

Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

11.64 0.53 ug/1 65846 1,4-Dichlorobenzene-d4 11.78

Hit# of 5 ‘entative ID MW MolForm CAS# Qual

1 1,4-Dichl6robenzene-d4 150 C6C12D4 003855-82-1 83 2 Benzenamine, 2-methyl-4-nitro- 152 C7H8N2O2 000099-52-5 22 3 Benze: imine, 2-methyl-5-nitro­ 152 C7H8N2O2 000099-55-8 22 4 Benz© .e-1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 17 *\bundance Scan 719 (11.643 min): 23082.D (-) m/z 149.90 ,100.00% i$o

5000 115 52 78 38 . 11.40 11.60 11.80 12.00 ........ Ill,,,,,,,,,,,,, 414^ m/z 151.90 , 58.42% m/z-> 30 40) 50 60 70 80 90 100 110 120 130 140 150 160 flibundance #9593: 1,4-Dichlorobenzene-d4 150

5000 115 78 11.40 11.60 11.80 12.00 52 m/z 115.00 , 35.97% I 35 I'I''''I' I

jm/z--> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #10129: Benzenamine. 2-niettiyl-4-nitro- 77 106 152

11.40 11.60 11.80 12.00 5000 m/z 78.05 19.71% 51 I

!, 66

m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 'Kbundance #66885: Benzenamine, 2-methyl-5-nitro- 77 106 152 11.40 11.60 11.80 12.00 m/z 52.00 , 14.33%

SEE 51 94

t m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.40 11.60 11.80 12.00

23082.D NP091101.M Tue Oct 09 12:23:32 2001 Page 2

NYC-WTC_000087883

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NYC-WTC_000087883Source: NYC Law Department, mirrored locally

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