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GC/MS analysis results for sample AD23833, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23833 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089461–000089475

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089474
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NYC 9/11 Public Portal Document » Library Search Compound^ Report Data File : C:\HPCHEM\1\DATA\OCT3001\23833.D Vial: 18 Acq On : 31 Oct 2001 7:06 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1,00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DAT7kBASE\NBS75K.L ********************************************************************* Peak Number 6 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.58- 0.53 ug/1 72346 1,4-Dichlorobenzene-d4 11-71 Hit# of 5 ntative ID MW MolForm CAS# Quai ; 1 1,4-Dichlo/bbenzene-d4 150 C6C1.2D4 003855-82-1 72 2 Benzene- y2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 -37 3 2-Methyl/6-nitroaniline 152 C7H8N2O2 000570-24-1 10 ' 4 Biphenyl ene 152 C12H8 000259-79-0 10 ■ Abundance 7 Scan 711 (11.576 min): 23833.D (-) m/z 149.90100400% 1!IO

5000 115 52 78 11.20 11.40 11.60 11.80 12.00

TiZz-> 20 40 '' ' ' I ' ' '-''I ' 30 40 utx4^ 50 60 70 80 90 100 110 120 130 140 150 160 ra/z 151.90 59.69% Abundance #9593:1.4-Dichlorobenzene-d4 1!!0

5000 115 78 11.20 11.40 11.60 11.80 12.00 52 m/z 115.00 . 41.79%

TiZz-> 20 » 30 35 40 ' I '' '• I ' '' 'I' 50 60 70 11 •''' I' 80 90 4^ 100 110 120 130 140 150 160 ■ Abundance #9592: Benzene-1,2.3,4<l4-, 5,&<iichloro 1!i0

115 11 20 11.40 11.60 11.80 12.00 5000 52 78 m7z 77.95 . 20.45%

_ _ _ _35_____ _-87___ .... I ' I''' ' r ' I' I'''' I 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #66883: 2-Methyl-6-n'itroaniline ~77“- " ■ 441 $2 4 “m/z 52.00 18.13%

5000 106 52 .J,.. I 20 ' ' 30 " 40 " 50 ' 60 70 80 90 94

^4^^^ 100 110 120 130 140 150 160 11.20 11.40 11.60 11,80 12.00

23833.D NP103001.M Thu Nov 01 13:18:33 2001 Page 6

NYC-WTC_000089474

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NYC-WTC_000089474Source: NYC Law Department, mirrored locally

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