Laboratory report documenting GC/MS analysis of sample AD23833 conducted on November 1, 2001, identifying unknown compounds.
NYC-WTC_000089461–000089475Folder label: “GC/MS Scan 10/1/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3001\23833.D Vial: 18 Acq On : 31 Oct 2001 7:06 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1’. 00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 1.26 ug/1 172698 1,4-Dichlorobenzene-d4 11.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 40 2 Morpholine, 4-methyl- 101 C5H11N0 000109-02-4 9 3 N,N' -/is(2-methyl-2-nitrosopentan-4 258 C12H22N2O4 094514-30-4 9 4 Acet/c acid, 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 9 Abundance ' Scan 288 (7.692 min): 23833. D (-) m/z 42.95 100.00% 4(3
253
Tlfe-> ' I " " I ..... . 10 20 30 40 50 53„ 59
60 71 ' I ' ' ' ' I 70 80 83 , ' I • ' '' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' 90 100 101
110 120 130 ■ "I TI r r
m/z^ 7.40 7.60 !59.05 L7.80 8.00 52.29% Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 4(3
5000 59 7.40 7.60 7.80 8.00 m/z 100.95 22.23% 27 101 ......J, ,1... I 83 1,1.,,,,.......... . ' I'''' I'''' I' Tife-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #1640: Morpholine.Amethyl- ' $
7.40 . 7.60 7.80 8.00 5000 m/z 58.05 16.07% 101 15 - I 27 56 71 —I--- ■n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #35454: N,N'-Bis{2-methyl-2-nitrosopentan-4-one) ---------------- -------------------- — r----------- I' I'1'-I 7.40 7.60 7.80 --8.00 --. ■ m/z 41.05 6.78%
fez: 5000
99 ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' 83 I 130 ■n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 7.40 7.60 7.80 8.00
23833.D NP103001.M Thu Nov 01 13:18:31 2001 Page 5
NYC-WTC_000089473
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NYC-WTC_000089446
Laboratory report documenting GC/MS analysis of sample AD23797 conducted on November 1, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089501
Laboratory report documenting GC/MS analysis of sample AD23835 conducted on November 1, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089115
Laboratory record for sample AD23656 showing detection of unknown compounds on October 16, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089203
Laboratory record for sample AD23719 showing detection of unknown compounds on October 17, 2001.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067675
DEP lab report for GCMS analysis of sample AD23948 conducted on October 25, 2001, noting unknown compounds.
1 shared non-person entities · 1 shared topics · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067796
Laboratory report documenting GCMS analysis of sample AD23998 conducted on October 29, 2001, noting unknown compounds.
1 shared non-person entities · 1 shared topics · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067811
Laboratory report documenting GCMS analysis of sample AD24046 conducted on October 29, 2001, noting unknown compounds.
1 shared non-person entities · 1 shared topics · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067826
Laboratory report documenting GCMS analysis of sample AD24047 conducted on October 29, 2001, noting unknown compounds.
1 shared non-person entities · 1 shared topics · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067752
Laboratory report documenting GCMS analysis of sample AD23995 conducted on October 29, 2001, noting unknown compounds.
1 shared non-person entities · 1 shared topics · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067908
Laboratory report documenting GCMS analysis of sample AD24133 conducted on October 29, 2001, noting unknown compounds.
1 shared non-person entities · 1 shared topics · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068748
Gas chromatography-mass spectrometry analysis of sample AD24482 completed November 13, 2001, identifying other unknown compounds with violations referenced in comments.
1 shared non-person entities · 1 shared topics · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067894
Laboratory report documenting GCMS analysis of sample AD24052 conducted on October 29, 2001, noting unknown compounds.
1 shared non-person entities · 1 shared topics · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000089273
Gas chromatography-mass spectrometry scan results recorded on October 1, 2001 for environmental samples.
Filed in the same folder
NYC-WTC_000089274
Detailed GC/MS calibration report for October 1, 2001, including peak data and method parameters.
Filed in the same folder
NYC-WTC_000089278
GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
Filed in the same folder
NYC-WTC_000089299
Laboratory record for sample AD23798 showing detection of unknown compounds on November 1, 2001.
Filed in the same folder
NYC-WTC_000089311
Laboratory report documenting GC/MS analysis of sample AD23799 conducted on November 1, 2001, identifying unknown compounds.
Filed in the same folder