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GC/MS analysis results for sample AD23833, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23833 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089461–000089475

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089472
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3001\23833.D Vial: 18 Acq On : 31 Oct 2001 7:06 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1,00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Hexanol Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.66 0.48 ug/1 66457 1,4-Dichlorobenzene-d4 11.71 Hit# of Tentative ID MW MolForm CAS# Qua! 1 2-Hexyhol 102 C6H14O 000626-93-7 83 2 2-Pe^anol, 4-methyl- 102 C6H14O 000108-11-2 74 3 2-^xanol, (S) - 102 C6H14O 052019-78-0 40 4 2-/entanol, 3-methyl-______________ 102 C6H14O 000565-60-6 39 “Sundance Scan 176 (6.664 min): 23833.D (-) m/z 457705 100.00% 4b

5000

■ r I'T I , I , , "Tt I I I I 41 6.40I 6.60 6.80 7.00 8487 III......... . ........ TTTTTT+hrkrrrTTTTrr m/z 69.00 14.59% nZz-> 10 15 20 25 30 35 '40 45 50 55 60 65 70 75 80 '85 90 95 Abundance #63584:2-Hexanol 4b

5000 4^ 6.40 6.60 6.80 7.00 69 "Wz 417705 12.86% 56 ......... TiZ2-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance#63545:2-Pentanol, 4-methyl-; , 4b

. ' 6.40 6.60 6.80 7.00 553 ^tn/z 43.05 11746%

69 -27— —394: r I""I""I .................... Ill I I' 11' " 111" I" " I " > 11' " > I • ■" I " 111 > 11111 ■ • ■ I • ■ nfe-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1769;2-Hexanol,(S)- "“4)5 .yoo'—Z m/z 44.00 9.17% 5000

55 y 8487 . TTpTTTyrTTTpTT-rpTT-hpTTTyrTTrpTTTp-T^^ Tnlz~> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 . 6.40 6.60 6.80 7.00

23833.D NP103001.M Thu Nov 01 13:18:29 2001 • Page 4

NYC-WTC_000089472

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NYC-WTC_000089472Source: NYC Law Department, mirrored locally

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