GC/MS analysis results for sample AD23085, Oct 2001

NYC 9/11 Public Portal Document

Data File C:\HPCHEM\1\DATA\OCT0401\23085.D Vial: 5 Acq On 4 Oct 2001 7:26 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library- : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,4-Dichlorobenzene-d4 Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

11.64 0.54 ug/1 75524 1,4-Dichlorobenzene-d4 11.78

Hit# of Tentative ID MW MolForm CAS# Qual

1 1,4-DAchlorobenzene-d4 150 C6C12D4 003855-82-1 94 2 Benztfne-l,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 40 3 Acenaphthylene 152 C12H8 000208-96-8 10 4 Benzaldehyde, 2-hydroxy-5-methoxy- 152 C8H8O3 000672-13-9 10 'Abundance Scan 719 (11.638 min): 23085.D (-) m/z 149.90 100.00% 1$0

5000 115 78 y J ,, 63 11.40 11.60 11.80 12.00 'r, I I , , l-l , I , I I I t+rp'r ' I ' ‘ ' I' ' ‘ ' I m/z 151.90 62.85% m/z-> 30 40__ 50___ 60 70 80__ 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichiorobenzene-d4 150

5000 115 78 11.40 11.60 11.80 12.00 52 m/z 114.90 . 35.98% I 35 .. ln/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 (Abundance #9592: Benzerie-1.2.3.4-d4-, 5.6-dichtoro- 150

115 11.40 11.60 11.80 12.00 5000 52 78 m/z 77.95 . 23.57%

35 87

mfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance ^7015: Acenaphthylene 152 11.40 11.60 11.80 12.00 m/z 75.90 , 12.46% 5000

...................... 87 98 126 T-t-r- 11 Ti/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.40 11.60 11.80 12.00

23085.D NP091101.M Tue Oct 09 12:31:08 2001 Page 1

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