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GCMS analysis results for sample AD24051, Oct 29 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24051 conducted on October 29, 2001, noting unknown compounds.

NYC-WTC_000067880–000067893

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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NYC 9/11 Public Portal Document

Library Search Confound Report Data Pile : C:\HPCHEM\1\DATA\OCT2501\24051.D Vial: 12 Acq On : 25 Oct 2001 11:26 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M {RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.59 0.57 ug/1 112872 1,4-Dichlorobenzene-d4 11.73 Hit# of 5 'entative ID MW MolForm CAS# Qual 1 1,4-Dich^robenzene-d4 150 C6C12D4 003855-82-1 78 2 Benzene^A,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 25 3 2-Meth^-6-nitroaniline 152 C7H8N2O2 000570-24-1 10 4 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 Abundance Scan 713 (11.593 min): 24051 .D (-) Tm/z 149.90 100.00% 1!0

5000 115

52 78 ,, R 1120 11.40 11.60 11.80 12.00 38 '' l-t"'' ■' 1-1+^ 87 rWyr I ' I'''' I m/z 151.90 . 62.86% TiZz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 Ito

5000 115 J 78 11.^ 11.40 11.60 11,80 12.00 52 m/z 114.90 . 39.90%

TiZz-> 20 30 35 40* " 50 ..... 11,..%. 100 110 120 130 140 150 1M 60 70 80 90 - Abundance #9592: Benzene-1.2,3.4-d4-, 5,Michlort> 1!0 _ 1 5 11.^ 11.40 11.60 11.80 12.00 5000 52 78 m/z 78.05 21.84%

87 35 I I ' I''' ‘ I' A u ' i ‘ ‘ ' I ’ Tlfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #86883:2-Methyl-6-nitroaniline T T 77 1!i2 11.^ 11.40 11.60 11.80 12.00 m7z 52.00 16.63%

5000 106

ttZz-> 20 ux J 30 40 50 60 70 80 90 94

100 110 120 130 140 150 160 I ‘ ‘ I ' ' ' ' 1 ' ' 11.20 11.40 11.60 11.80 12.00

24051.D NP101901.M Fri Oct 26 10:29:33 2001 Page 5

NYC-WTC_000067892

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NYC-WTC_000067892Source: NYC Law Department, mirrored locally

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