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GCMS analysis results for sample AD24051, Oct 29 2001

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Laboratory report documenting GCMS analysis of sample AD24051 conducted on October 29, 2001, noting unknown compounds.

NYC-WTC_000067880–000067893

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT2501\24051.D Vial: 12 Acq On : 25 Oct 2001 11:26 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method ; C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L A******************************************************************** Peak Number 4 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.73 1.28 ug/1 255355 1,4-Dichlorobenzene-d4 11.73 Hit# of 5 'entative ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 47 2 Morpholinte, 4-methyl- 101 C5H11N0 000109-02-4 9 3 3-Hydr. -2-pentanone 102 C5H10O2 003142-66-3 9 4 Acetip acid, cyano-, 1,1-dimethylet 141 C7H11N02 001116-98-9 9 Abundance 4 Scan 292 (7.728 min): 24051 .D (-) Tm/z 42.95 100.00% 413

59 5000 101 T 7.40 7.60 Tso 8.00 ......................... 38.1 71 83 I ' ' ' ' i ' ' ' ' I ' ' ' ' I r-j—r-i—r-r-]—1 I r' I I ' I 1 m/z 59.05 54.88% ■nfe-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64274:2-Pentanone, 4-hydroxy-4-methyU 43

5000- T 59 7.40 7.60 7.80 8.00 m/z 101.05 23.35% 27 101 .......................... I I ................................. 1,1.............. Tife-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1640: Morpholine, 4-methyl- 4|3

7.40 7.60 7.80 8.00 252 m/z 58.05 17.22% 101

■nfe-* Abundance 10 Lx 20 30 I 56 n~ I ' ' I ‘ ‘ I ‘ I 40 50 60 71 r-fL-i-r-rYT-r-r-i-p-T-T-r-fL-rr-T^

70 #1691:3-Hydroxy-2-pentanone 80 90 100 110

3(1 5? 7.40 7.60 7.80 8.00 ra/z 41.05 8.50% 5000 45 15 , , J...... II..... I ' ' ' ' I ' ‘ ' I ‘ ‘ ' I , ||, .«5, y?,, y.............. I ■ I ■ •nfe-> 10 2) 30 40 'sb' ‘ eo’ " 70 ' ao''' '90' ' '160 ' 116 7.40 7.60 7.80 8.00

24051.D NP101901.M Fri Oct 26 10:29:24 2001 Page 4

NYC-WTC_000067891

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NYC-WTC_000067891Source: NYC Law Department, mirrored locally

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