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GC/MS analysis results for sample AD22654, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22654 conducted on October 12, 2001, noting other unknown compounds.

NYC-WTC_000087463–000087490

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087473
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NYC 9/11 Public Portal Document

Library Search Compound Report ■ Data File : C:\HPCHEM\1\DATA\OCT1101\22654.D Vial: 6 ' Acq On : 11 Oct 2001 2:38 pm Operator: 2 09 GTkLOS Sample : reinject Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library ; C:\DATABASE\NBS75K.L Peak Number 2 2-Hexanone Concentration Rank 15 R.T. EstConc Area Relative to ISTD R.T. 6.48 0.78 ug/1 100422 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 ;ntative ID MW MolForm CAS# Qual 1 2-Hexanoni 100 C6H12O 000591-78-6 91 2 2-Hexanonl , 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 83 3 Oxirane/ :2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 72 4 Methyl/Isobutyl Ketone 100 C6H12O 000108-10-1 58 Abundance 7 Scan 156 (6.476 min): 22654.D (-) m/z 47795 100.00% 43

58 5000

I 71 85 100 6.20 6.40 6.60 6.80 5,^ "l I ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ‘ ‘ ' I ' mZz 58.05 51.60% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #63384: 2-Hexanone 43

5000 58 6.20 6.40 6.60 6.80 29 m/z 57700 18.23%

n/z-> 20 LX 30 40 50 .1,, 60 70 80 90 100 110 120 130 140 Abundance #11968: 2-Hexanone, 4-hydroxy-3-propyl- 43

58 6.20 6.40 6.60 6.80 5000 29 m/z 41.05 16.62%

Tl/z-> H ' ' ' ' I ' ' ' ' I I 20 30 40 ,1, ' I ‘ ' ' I I ' 50 60 70 80 71

90 85

100 110 120 100

130 140 140 Abundance #1530: Oxirane, 2-methyl-2-(1-methylethyl)- 43 6.20 6.40 6.60 6.80 58 m/z 100.05 10.34% II 5000 71

30 85 100 ■n/z-> "I-' '"I........... 20 30 40 .Mr 50 60 70 80 ■I I 90 I 100 I 110 120 130 140 6.20 6.40 6.60 6.80

22654.D NP091101.M Fri Oct 12 09:09:05 2001 Page 2

NYC-WTC_000087473

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NYC-WTC_000087473Source: NYC Law Department, mirrored locally

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