GCMS reference analysis results for sample AE07311, April 2002

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\APR0302\1965.D vial: 6 Acq On 3 Apr 2002 5:35 pm Operator: Sample re-extract Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0403.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 2-Hexanone Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

6.95 1.03 ug/1 113344 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexanone 100 C6H120 000591-78-6 91 2 2-Hexanone, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 83 3 Oxirane, 2-methyl-2-(1-methylethyl) 100 C6H120 072221-03-5 72 4 Methyl Isobutyl Ketone____________ 100 C6H120 000108-10-1 53 Abundance Scan 208 (6.952 min): 1965.D (-) m/ z 43.05 100.00% 43

58 _......... _ 5000

। । । I I r t । । । । । । । । । । । । 1/d/)T 100

m/z-> 20 —l 30 40 51 TIT 50 60 70 71

80 85 ' i • ■ ' ■ i 1' 1 ' 1 i ■ ■ 1 ' ■ I ■ 90 100 110 120 130 140 660 m/z 6.80 58.05 7.00 7.20 56.65% Abundance #63386: 2-Hexanone 43

A / 3------ — 5000 58 660 6.80 7.00 7.20 29 m/z 56.95 18.22% 71 85 100 I ■ ' 1 1 i ■ 1 ' 1 i ' ' 1 1 i ' -------------------- 1 i ■ ■11 i r 1 ■ 1 । । 1 i ' 1 m/z->_ 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #11968: 2-Hexanone, 4-hydroxy-3-propyl- 43

58 6.60 6.80 7.00 7.20 5000 29 m/ Z 41.05 16.24%

/z-> Abundance 20 ■ ।11 1 I ' ' ' ' I I.......... 30 40

43 50 60 71 I 85 I 1 1 1 1 i ' ■ r ■ ।' ■ ■' ।'1 70 80 100 140 I I I I I I I I I I I I j ~r l ~ T I ' I” I I

90 100 110 120 130 140 #1530: Oxirane, 2-methyl-2-(1-methylethyl)- 660 r 6.80 U 7.00 7.20

i 58 m/z 100.05 11.64% 5000 71

30 52 85 100 ^1 1 ' 1 1 I 1 1 1 1 1 1 1...... . ----------------- ’ 11’111+1*1 i 1 1 1 ' i ' m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 6.60 6.80 7.00 7.20

1965.D GCMS0403.M Tue Apr 09 13:07:24 2002 Page 2

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