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GC/MS analysis results for sample AD22654, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22654 conducted on October 12, 2001, noting other unknown compounds.

NYC-WTC_000087463–000087490

Folder label: “GC/MS Scan 9/19/01

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NYC 9/11 Public Portal Document

Library Search Compound Report ■ Data File : C:\HPCHEM\1\DATA\OCT1101\22654.D Vial: 6 Acq On : 11 Oct 2001 2:38 pm Operator: 209 GALOS Sample : reinject Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★ Peak Number 1 Oxirane, tetradecyl- Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 5.13 3.68 ug/1 477058 1,4-Dichlorobenzene-d4 11.76

Hit# of 5 Ten tive ID MW MolForm CAS# Qual

1 Oxirane, tet decyl- 240 C16H32O 007320-37-8 27 2 1*2-Cycloh.yicanediol, 1-methyl-, tra 13 0 C7H14O2 019534-08-8 14 3 17-Penta Ziacontene 491 C35H70 006971-40-0 10 4 4,5-Oct edione 142 C8H14O2 005455-24-3 10 Abundance Scan 9 (5.126 min): 22654.D (-) 100.00% 105 41 71

175 5000

217 260 5.10 5.20 5.30 5.40 5.50

Tl/Z-> 50 100 150 MtU 200 250 300 350 400 450 m/z 41.05 80.77% Abundance #71188: Oxirane, tetradecyl- 41 71

97 5000 T 5.10 5.20 5.30 5.40 5.50 125 m/z 71.00 76.72%

Ti/z-> c 50.J U,100 150 200 2^ ..................... ' 300 350 400 450 Abundance #5409: 1,2-Cyclohexanediol, 1-methyl-, trans- 71

5.10 5.20 5.30 5.40 5.50 5000 m/z 43.05 73.94%

—^112 1)1, ,1,1..... ..... ...... n/z-> 50 100 150 200 250 300 350 400 450 ^bundance #58705:17-Pentatriacontene 43 5.10 5.20 5.30 5.40 5.50 m/z91700 65.44%

5000 83

m/z-> 50 1,,1 1 1^39 ......................... .... 462 4^ 100 p-T-T-T-T-r-TTT-T-yT-T-T-r-^ 150200 250 300 350 400 450 5.10 5205^ 5.40 5.50

22654.D NP091101.M Fri Oct 12 09:09:03 2001 Page 1

NYC-WTC_000087472

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