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GC/MS analysis results for sample AD22654, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22654 conducted on October 12, 2001, noting other unknown compounds.

NYC-WTC_000087463–000087490

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087474
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NYC 9/11 Public Portal Document

Library Search Compound Report ■ Data File ; C:\HPCHEM\1\DATA\OCT1101\22654.D Vial: 6 Acq On : 11 Oct 2001 2:38 pm Operator: 209 GALOS Sample : reinject Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L Peak Number 3 2-Hexanol Concentration Rank 17 R.T. EstConc Area Relative to ISTD R.T. 6.72 0:50 ug/1 64962 1,4-Dichlorobenzehe-d4 11.76

Hit# Of 5 intative ID MW MolForm CAS# Qual

1 2-Hexano^ 102 C6H14O 000626-93-7 83 2 2-Pentanol, 4-methyl- 102 C6H14O 000108-11-2 78 3 2-Hex^l, (S)- 102 C6H14O 052019-78-0 43 4 2-Hey&nol, (R) -________________________ 102 C6H14O 026549-24-6 43 Abundance / Scan 183 (6.723 min); 22654. D (-) m/z 44795 100.00% 4^ I 5000

, , , 69

Tife-> Abundance 10 15 20 25 30 35 41 53 56 ■ifJ+U ''"I"" I II" I 40 45 50 55 60 65 #63584; 2-Hexanol a 70 75 T 8487 ' I' " 11' I' ’ I'''' I' 80 85 90 95 m/z 6.40 6.60 69.00 6.80 7.00 15.17%

5000 4$

“mTz ............A,') I 6.40 6.60 417705 u 6.80 7.00 13713% a 69 19 2/31 4^1 56 8487 ■prTTrpTTTiTMfmrrrrTr^ ' ' ............ I I'M I .......... I "T n/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1773; 2-Pentanol, 4-methyl- 4h3 T 6.40 6.60 6.80 7.00 5000 m/z 43.00 9.84%

27 69 42 I 8487 11111.. 111111.1111.. 1111.111.. 111.. 111.11

•n/z-> Abundance 10 15 20 25 30 35 40 45 50 55 60 65 70 75 #1769; 2-Hexanol, (S)- 4& 80 85 90 95 jy 6.40 6.60 6.80 7.00

s m/ z 44.00 8.92%

5000-

69 55 8487 I'''' 1' TM^H ‘' I'''' I •n/z~> 10 15 20 25 30 35 40^45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.00

22654.D NP091101.M Fri Oct 12 09:09:07 2001 Page 3

NYC-WTC_000087474

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NYC-WTC_000087474Source: NYC Law Department, mirrored locally

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