Instrument data sheet containing operational parameters and sample details for GCMS analysis conducted on October 15, 2001.
NYC-WTC_000068724–000068736Folder label: “GCMS Scan X 10/15/01 A 11/3/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : M:\INSTRU~1\209\DATA\OCT1801\LB.D Vial; 2 Acq On : 18 Oct 2001 5:09 pm Operator; 209 GALOS Sample : lab blk 10/15 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.48 1.07 ug/1 103630 1,4-Dichlorobenzene-d4 11.77
Hit# of 5 'entative ID MW MolForm CAS# Qual
1 2-Hexanone 100 C6H12O 000591-78-6 91 2 2-Hexanone, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 74 3 Methyl Isobutyl Ketone 100 C6H12O 000108-10-1 47 4 Propanal 58 C3H6O 000123-38-6 47 Abundance Scan 157 (6.479 min); LB.D (-) m/z 42.95 100.00% 43
58 5000
71 85 100 6.20 6.40 6.60 6.80 L I I m/z 58.05 55.70% Ti/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #63384: 2-Hexanone 43
5000 58 6.20 6.40 6.60 6.80 29 m/z sYToo 16.32% ,1 I, 71 85 100 ft 7i/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #11968:2-Hexanone, 4-hydroxy-3-propyl- 43
58 6.20 6.40 6.60 6.80 5000 29 “m/z 41.05 15.25%
.........'''I............ J. 71 I 140 ■nfz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #1526: Methyl Isobutyl Ketone 4)3 6.20 6.40 6.60 6.80 m/z 100.00 10.69% 5000 58 27 85 100 51 . , ,67..... ,, ,1, ,,,,,, I........... ....... ......... A
•nfe~> 20 30 40 50 60 70 80 90 100 110 120 130 140 6.20 6.40 6.60 6.80
LB.D NP103001.M Fri Nov 09 16:25:11 2001 Page 2
NYC-WTC_000068731
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NYC-WTC_000068432
Laboratory report documenting GCMS analysis of sample AD24472 conducted on November 14, 2001, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068559
Calibration data table for GC/MS instrument used in TCLP analysis, generated on November 5, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067428
Laboratory report detailing GCMS analysis of sample AD22558 conducted on October 1, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067739
Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 25, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067979
Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.986
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068400
Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.986
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069732
Calibration table listing standard compounds and response values for GCMS analysis dated November 16, 2001.
1 shared topics · Same agency, volume and box · similarity 0.985
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067623
DEP lab report for GCMS analysis of sample AD23914 conducted on October 25, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.985
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067555
DEP lab report for GCMS analysis of sample AD23909 conducted on October 23, 2001, noting unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.984
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088491
Calibration data table for TCLP analysis using GC/MS standards processed on October 18, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089030
GC/MS analysis report with TCLP calibration table data from October 16, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.987
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017126
Laboratory report documenting GCMS analysis of sample AD30601 for volatile organic compounds on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.984
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000068720
Record of a GCMS scan conducted at the World Trade Center site in mid-November 2001.
Filed in the same folder
NYC-WTC_000068721
Document page containing identification codes for GCMS scans conducted in November 2001 within DEP Box 60.
Filed in the same folder
NYC-WTC_000068737
Laboratory report documenting GCMS analysis of sample AD24333 with detection of unknown compounds on November 27, 2001.
Filed in the same folder
NYC-WTC_000068748
Gas chromatography-mass spectrometry analysis of sample AD24482 completed November 13, 2001, identifying other unknown compounds with violations referenced in comments.
Filed in the same folder
NYC-WTC_000068763
Laboratory report documenting GCMS analysis of sample AD24483 identifying unknown compounds on November 13, 2001.
Filed in the same folder