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GCMS analysis results for sample AD24472, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24472 conducted on November 14, 2001, identifying unknown compounds.

NYC-WTC_000068432–000068446

Folder label: “GCMS Scan X 10/12/01 An 11/3/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\OCT1601\24472.D Vial: 17 Acq On : 17 Oct 2001 5:53 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L Peak Number 2 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.49 1.13 ug/1 109096 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexan^e 100 C6H12O 000591-78-6 91 2 Methy^z^sobutyl Ketone 100 C6H12O 000108-10-1 58 3 Prop^al 58 C3H6O 000123-38-6 43 4 2-Hexanone, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 39 Abundance Scan 158 (6.488 min): 24472.D (-) m/z 42.95 100.00% 4(3

58 5000

6.20 6.40 6.60 6.80

Tife-> I ' Tpn j . (h.. T.. T. 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 m/z 58.05 A 55.82% Abundance #63387:2-Hexanone 43

58 5000 6.20 6.40 6.60 6.80 100 m/z 41.05 15.34% I'' " I''' 'T I TTTpil+pTTTY'TTTyl-rrTpTT-^^ T " I" " '"' I" " I tVz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63350: Methyl Isobutyl Ketone 4(3

6.20 6.40 6.60 6.80 5000 m/z sYTOO 14.68% 58

85 100 27 67 .. I'l'.... I|'l . . . 'I" "I'"'I Tife-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #97: Propanal 23 _6jo__6xg_a6g__6,8o__ m/z 100.05 11.87% 58 5000

, ? 44 .. I'''' I'''' I ■n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80

24472.D NP103001.M Fri Nov 09 11:44:35 2001 Page 2

NYC-WTC_000068441

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NYC-WTC_000068441Source: NYC Law Department, mirrored locally

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