GCMS analysis results for sample AD24472, Nov 2001

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Data File : M:\INSTRU~1\209\DATA\OCT1601\24472.D Vial: 17 Acq On ; 17 Oct 2001 5:53 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C;\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 6.62 0.46 ug/1 44695 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanox 102 C6H14O 000623-37-0 78 2 Butane/^ -methoxy- 88 C5H12O 006795-87-5 38 3 3-Pe;H^nol 88 C5H12O 000584-02-1 36 4 3-J>entanol, 2-methyl- 102 C6H140 000565-67-3 36 ftbundan^e Scan 172 (6.617 min); 24472. D (-) m/z 59.05 100.00% 55 5b

50)0 73

43 ■ I , Cl J 39 6.20 6.40 6.60 6.80 7.00 -rp-rr -i4+ 'I"" I"''I" "I"" I " m/ z 54.95 86.30% mfe-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63531:3-Hexanol

55

5000 73 6.20 6.40 6.60 6.80 7.00 43 m/z 73.00 49.03% 39 44+ h '''' I'''' I'''' I''" I' ‘ mZz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #854: Butane, 2-methoxy- 5|9

....... ... 6.20 6.40 6.60 6.80 7.00 5000 m/z 42.95 25.05% A 15 ^^31 45 73 56 Tl/Z-> 5 " " I'' 4^ 7+++ 88 I " " I' 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #851:3-Pentanol 5i9 6.20 6.40 6.60 6.80 7.00 m/z 41.05 23.42% 31 5000 27 41 15 45

Tife-> 5 10 t+ 38 4^ I'''' I'''' 1'''' I 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.20 6.40 6.60 6.80 7.00

24472.D NP103001.M Fri Nov 09 11:44:40 2001 Page 3

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