GCMS analysis results for sample AD24472, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\OCT1601\24472.D Vial: 17 Acq On : 17 Oct 2001 5:53 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C;\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Hexanol Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 6.74 0.61 ug/1 59000 1,4-Dichlorobenzene-d4 11.77

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 2-Hexa: 1 102 C6H14O 000626-93-7 74 2 2-Pep>"danol, 4-methyl- 102 C6H14O 000108-11-2 74 3 2- nit anol 74 C4H10O 000078-92-2 50 4 lutanol, (R)- 74 C4H10O 014898-79-4 38 Abundance Scan 185 (6.736 tnin): 24472.D (-) Wz 45.05 100.00% 4|5

5000

41 69

Tlfe-> Abundance 10 15 20 25 30 ...... J.|||... 35 40 45 50 56

55 60 65 #63582: 2-Hexanol a 70 75 84 87 yTrr4-|-,l . r|- 80 85 90 95 ■p’ _640__a60__6;80__7t0__ Wz 69.10 16.50%

4|5

5000 ...................................................... 6.40 6.60 6.80 7.00 27 Wz 41.05 15.60% 69 19 31 1 57 I 8487 I " " I " '' I' " I' " I'•"IIII1I■."IH.II..IIII ■I■I■"II■I■■II,.,I, tVz~> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63546: 2-Pentanol, 4-methyl- 4^ .. I .... I 6.40 6.60 6.80 7.00 5000 m/z 43.05 10.94%

27 J 19 I 31 4^ T 84 8/ . ........... . '' I'''' 111'' I'''' I''' 11'''' I'''' I''' 11' I'' I'''' I' Ti^-> Abundance 10 15 20 25 30 35 40 45 50 55 60 65 #62568: 2-Butanol 415 70 75 80 85 90 95 Aj - I ' ' ' ' I ' ' ' ' I 6.40 6.60 6.80 7.00 m/z 43.90 10.06%

5000

27 31 59

Ti/z-> 10 15 20 25 Xuu 30 35 40 45 50 55 60 65 70 75 56 72 P" I' ‘' 1'''' I'''' I 80 85 90 95 6.40 6.60 ........................ 6.80 7.00

24472.D NP103001.M Fri Nov 09 11:44:44 2001 Page 4

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