Instrument data sheet containing operational parameters and sample details for GCMS analysis conducted on October 15, 2001.
NYC-WTC_000068724–000068736Folder label: “GCMS Scan X 10/15/01 A 11/3/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\OCT1801\LB.D Vial: 2 Acq On : 18 Oct 2001 5:09 pm Operator: 209 GALOS Sample : lab blk 10/15 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library ; C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 6.62 0.47 ug/1 45594 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-HexanDl 102 C6H14O 000623-37-0 74 2 3-Pentanol 88 C5H12O 000584-02-1 42 3 2,3/^utanediol, 2,3-dimethyl- 118 C6H14O2 000076-09-5 42 4 3-pentanol, 2-methyl- 102 C6H14O 000565-67-3 38 ^bundapfce Scan 172 (6.616 min): LB.D (-) m/z 59.05 100.00% sp
73 SHE 43 , I ,/>, TVYy-, , , p-r- 6.20 6;4g a60 6J0^W prrllW+hTTTTTr 4+ ........... ..................... 100.............. m/ z 55.00 82.52% •n/z-> Abundance 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 #63530: 3-Hexanol 5b I 73 5000 6.20 6.40 6.60 6.80 7.00 31 m/z 73.00 50.10% 45 I" " 111" I ''' I *f--r 4 I............I 11' ’'' 11 ''841111 I. I n .«11 I.. I.. I. I. H n 11 Ti/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #62943:3-Pentanol 5b __ ...../ .3. V.......... 31 6.20 6.40 6.60 6.80 7.00 5000 Wz 42.95 28.95% 41
'' I'''' I' .. I " H I " 1 II I " . I II . II, , I ■ I■ I 1 , I I I ■ I I, I " I " ■ . I, I , I I , I Ti/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Naundance #64428:2,3-Butanediol. 2,3-dimethyl- 5b 6.20 6.40 6.60 6.80 7.00 ■m/z 41.00 28711%
5000 43
Tl/Z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.20 6.40 6.60 6.80 7.00
LB.D NP103001.M Fri Nov 09 16:25:15 2001 Page 3
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NYC-WTC_000068432
Laboratory report documenting GCMS analysis of sample AD24472 conducted on November 14, 2001, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068559
Calibration data table for GC/MS instrument used in TCLP analysis, generated on November 5, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067428
Laboratory report detailing GCMS analysis of sample AD22558 conducted on October 1, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067739
Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 25, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067979
Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.986
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068400
Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.986
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069732
Calibration table listing standard compounds and response values for GCMS analysis dated November 16, 2001.
1 shared topics · Same agency, volume and box · similarity 0.985
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067623
DEP lab report for GCMS analysis of sample AD23914 conducted on October 25, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.985
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067555
DEP lab report for GCMS analysis of sample AD23909 conducted on October 23, 2001, noting unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.984
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088491
Calibration data table for TCLP analysis using GC/MS standards processed on October 18, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089030
GC/MS analysis report with TCLP calibration table data from October 16, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.987
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017126
Laboratory report documenting GCMS analysis of sample AD30601 for volatile organic compounds on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.984
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000068720
Record of a GCMS scan conducted at the World Trade Center site in mid-November 2001.
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Document page containing identification codes for GCMS scans conducted in November 2001 within DEP Box 60.
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NYC-WTC_000068737
Laboratory report documenting GCMS analysis of sample AD24333 with detection of unknown compounds on November 27, 2001.
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NYC-WTC_000068748
Gas chromatography-mass spectrometry analysis of sample AD24482 completed November 13, 2001, identifying other unknown compounds with violations referenced in comments.
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Laboratory report documenting GCMS analysis of sample AD24483 identifying unknown compounds on November 13, 2001.
Filed in the same folder