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GCMS analysis results for sample AD24698, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24698 identifying unknown compounds on November 19, 2001.

NYC-WTC_000068853–000068865

Folder label: “GCMS Scan X 10/17/01 An 11/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0501\24698.D Vial: 19 Acq On 6 Nov 2001 5:31 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanol Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.67 0.45 ug/1 70393 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexapdl 102 C6H14O 000626-93-7 83 2 2-Pentunol, 4-methyl- 102 C6H14O 000108-11-2 74 3 2-B )^anol, (R) - 102 C6H14O 026549-24-6 64 4 2/P entanol, 3-chloro-4-methyl-, (R® 136 C6H13C1OI 074685-47-5 40 Abundance Scan 177 (6.667 tnin): 24698.D (-) m/z 45.05 100.00%) 4)5

5000

41 69 . , I ‘ I IVn-T-r, ■ 1 . 51 ^59 ) 8487 6.40 6.60 6.80 7.00

n/z-> ,....„a,liil I *' " I ‘ ‘ ' I'' ‘ * I 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 m/z 41.00 15771% Abundance #63583:2-Hexanol 4)5

5000 TT-T-T-yT-T-T-T-yT-T-T-T-yT-T-TT^^ 6.40 6.60 6.80 7.00 m/z 69.00 14.86% 69 ) 8487 " I" ‘' I" " I" ‘' I"'' I' I" I" " I' T)Zz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85K)95 Abundance #1773:2-Pentanol, 4-methyl- 4)5 A. / i A , , , / ' ' ' 6.^16.^' 6.^ 7.ro' 5000 m/z :43.90 14.83%

27 69 42 I 8487 Tlfe-> T An l-rnTrT-rrrH+rTTTTTTTT^^ 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1794:2-Hexanol. (R)- 4b 6.40I 6.60 6.80 7.00 in/z 43.05 12.73% 553

Tlfe-> 19 M 55 69 ^42, I 8487 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 ■ ■ I “ ■ ■ I" “ I" ‘' I ■ ‘" I • “ ■ I" • • I ■' “ I “ ‘' I ■ JU 6.40 6.60 6.80 7.00

24698.D NP103001.M Tue Nov 13 12:06:49 2001 Page 2

NYC-WTC_000068862

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NYC-WTC_000068862Source: NYC Law Department, mirrored locally

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