Instrument data sheet containing operational parameters and sample details for GCMS analysis conducted on October 15, 2001.
NYC-WTC_000068724–000068736Folder label: “GCMS Scan X 10/15/01 A 11/3/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : M:\INSTRU"1\2 0 9\DATA\OCT18 01\LB.D Vial: 2 Acq On : 18 Oct 2001 5:09 pm Operator: 209 GALOS Sample : lab blk 10/15 Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C;\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.37 0.47 ug/1 45805 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Hexanphe 100 C6H12O 000589-38-8 90 2 3-Pentanone, 2-methyl- 100 C6H12O 000565-69-5 47 3 3-Buten-2-ol 72 C4H8O 000598-32-3 38 4 2,4-Pentanedione 100 C5H8O2 000123-54-6 35 Abundance Scan 145 (6.368 min): LB.D (-) m/z 43.05 100.00% 43 57
71 220 100 ....... 6 00 6.20 6.40 6.60 6.80 85 m/z 57.00 88773% jTTTTp-rnj t I '' ' ' I I ‘' r''' I"'' I ■n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1528: 3-Hexanone 43 57
29 71 5000 6.00 6.20 6.40 6.60 6.80 100 m/T 71.00 55.02% ■ ..... '"I ... tVz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63399:3-Pentanone. 2-methyl- 43 5|7
6.00 6,20 6.40 6.60 6.80 c 220 m/z 100.0531.95% 71 100 I A 85 +-T nyz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #62480:3-Buten-2-ol _\, A.... I ,,, I, 5(7 __6W_620__640_6,60__6^ 43 “m/z 41.00 25752%
222 27
t+ —- I'''' I'' " I'''' I ■n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.00 6.20 6.40 6.60 6.80
LB.D NP103001.M Fri Nov 09 16:25:06 2001 Page 1
NYC-WTC_000068730
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NYC-WTC_000068432
Laboratory report documenting GCMS analysis of sample AD24472 conducted on November 14, 2001, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068559
Calibration data table for GC/MS instrument used in TCLP analysis, generated on November 5, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067428
Laboratory report detailing GCMS analysis of sample AD22558 conducted on October 1, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067739
Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 25, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067979
Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.986
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068400
Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.986
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069732
Calibration table listing standard compounds and response values for GCMS analysis dated November 16, 2001.
1 shared topics · Same agency, volume and box · similarity 0.985
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067623
DEP lab report for GCMS analysis of sample AD23914 conducted on October 25, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.985
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067555
DEP lab report for GCMS analysis of sample AD23909 conducted on October 23, 2001, noting unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.984
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088491
Calibration data table for TCLP analysis using GC/MS standards processed on October 18, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089030
GC/MS analysis report with TCLP calibration table data from October 16, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.987
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017126
Laboratory report documenting GCMS analysis of sample AD30601 for volatile organic compounds on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.984
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000068720
Record of a GCMS scan conducted at the World Trade Center site in mid-November 2001.
Filed in the same folder
NYC-WTC_000068721
Document page containing identification codes for GCMS scans conducted in November 2001 within DEP Box 60.
Filed in the same folder
NYC-WTC_000068737
Laboratory report documenting GCMS analysis of sample AD24333 with detection of unknown compounds on November 27, 2001.
Filed in the same folder
NYC-WTC_000068748
Gas chromatography-mass spectrometry analysis of sample AD24482 completed November 13, 2001, identifying other unknown compounds with violations referenced in comments.
Filed in the same folder
NYC-WTC_000068763
Laboratory report documenting GCMS analysis of sample AD24483 identifying unknown compounds on November 13, 2001.
Filed in the same folder