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GCMS analysis results for sample AD24472, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24472 conducted on November 14, 2001, identifying unknown compounds.

NYC-WTC_000068432–000068446

Folder label: “GCMS Scan X 10/12/01 An 11/3/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\OCT1601\24472.D Vial: 17 Acq On : 17 Oct 2001 5:53 am Operator: 209 GALOS Sample ; gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L Peak Number 1 3-Hexanone Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

6.38 0.52 ug/1 50873 1,4-Dichlorobenzene-d4 11.77

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexa: •ne 100 C6H12O 000589-38-8 90 2 Buta: , 2,2- dimethyl - 86 C6H14 000075-83-2 36 3 He; 4he, 3,3,4-trimethyl- 128 C9H20 016747-31-2 36 4 2 -Pentanedione 100 C5H8O2 000123-54-6 35 4bundaftce Scan 146 (6.378 min): 24472.D {-) m/z 43700 100.00% 43 57

71 5000 100

6.00 6.20 6.40 6,60 6,80 85 ...................... m/z 57.00 85.91% rVz-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #63358; 3-Hexanone

7^ 57

71 223 6.^ 6.20 6.^ 6.^ 6.M 100 m/z 71.00 61.35%

Tlfe-> 10 20 30 4 40 ' I ' ' ' ’'i ' 50 60 70 80 90 100 110 120 Abundance #732: Butane. 2,2-dimethyl- 4)3 517 71 6.00 6.20 6.40 6.60 6.80 29 m/z 100.05 31.48% 223 \

JyL 15 I ' I ' ' ' ‘I' ''' I I ^-l" " t'l ' ' '50' ' ttZz-> 10 20 30 40 60 70 80 90 100 110 120 ^bundance #5135: Hexane, 3,3,4-trimethyl- \ 43 57 71 6.00 620 6X0 6.60 6.80 m/z 41.00 28.79%

5000

27 99 ■ I ' I ' ' I ' ' ' ' I I I ■ 1 I I I 113 ' 1 I ' I ' ■nlz-> 10 20 30 40 50 60 70 80 90 100 110 120 6.00 6.20 6.40 6.60 6.80

24472.D NP103001.M Fri Nov 09 11:44:31 2001 Page 1

NYC-WTC_000068440

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NYC-WTC_000068440Source: NYC Law Department, mirrored locally

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