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GCMS analysis results for sample AD24133, Oct 29 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24133 conducted on October 29, 2001, noting unknown compounds.

NYC-WTC_000067908–000067921

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT2501\24133.D Vial: 14 Acq On : 26 Oct 2001 1:24 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method ; C:\HPCHEM\1\METHODS\NP101901.M {RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L Peak Number 1 3-Hexanone Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.36 0.43 ug/1 79220 1,4-Dichlorobenzene-d4 11.73 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hexa: me 100 C6H12O 000589-38-8 72 2 3-Pen' mone, 2-methyl- 100 C6H12O 000565-69-5 53 3 2,4- mtanedione 100 C5H8O2 000123-54-6 46 4 But e, 2,2-dimethyl-___________ 86 C6H14 000075-83-2 40 Abundance/ Scan 144 (6.362 min): 24133.D (-) m/z43.05 100.00% 4)3 57

71 5000

50 +nTTTrpT^ 85 100

"m/^ 6.00 6.20 57.00 AU-, 6.^' 6.60 ‘IS 90.55% 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63357:3-Hexanone 43 57 29 ..... 500) 71 6.00 6.20 6.40 6,60 6.80 100 71.00 56.25% ................I I’‘ •I”••1 .... . F”'!' ■nfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63398:3-Pentanone, 2-methyl-

43 5|7

600 6.20 A/L; 6.40 6.60 6.80 5000 m/z 100.05 39.23% 100 I I . X 71 85 ■nZz-> 20^ 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Mxindance #63324:2.4-Pentanedione ■ I 43 6.00 6,20 6.40 6.60 6.80 m/z 41.00 26.39% 5000 85 100

2/ 38 H 58 72 111 • I. j 1111 ] M fl JI lYi j 1111111 rrj J11«IIII»1111 rj 1111J1111 j»J1111 H I 1111 11111 j 1111 111 rj r i p 'nfe-> 20^ 30 35 40 45 50 55 60 65 70 75 80 85 90 100105 6.00 6.20 6.40 6.60 6,80

24133.D NP101901.M Fri Oct 26 10:35:17 2001 Page 1

NYC-VVTC_000067916

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NYC-WTC_000067916Source: NYC Law Department, mirrored locally

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