GCMS analysis results, sample AD25603, Nov 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV1601\25603.D Vial: 2 Acq On : 16 Nov 2001 4:00 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P Quant Method ; C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 1 3-Hexanone Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.32 0.40 ug/1 74419 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hexanon^ 100 C6H12O 000589-38-8 91 2 Pentane,3,4- trimethyl - 114 C8H18 000565-75-3 40 3 2,4-Pi'eatftanedione 100 C5H8O2 000123-54-6 38 4 ButaXe, 2,2-dimethy1- 86 C6H14 000075-83-2 36 Abundance ‘ Scan 139 (6.317 min): 25603.D (-) m/z 43.05 100.00% 43 57

71 5000

51 100

6.00 m/z J6.20 57.00 6.40 T 6.60 81.91% T

i'-— TiZz-> 20 30 40 50 70 80 90 100 110 120 ^bunebnee #63358: S-Hexanone 43 57

71 5000 ''e.bo ‘e.^' 6.^''e.CT 100 m/z 71.00 58.59% I'' I +V n/z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #64229: Pentane, 2,3,4-trimethyl- 43 71 6.00 6,20 6.40 6.60 5000 m/z 100.05 36.26%

27 55 I ' I I ‘ ‘ ' 1 ‘ ' 1 114 Tife-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #63324:2,4-Pentanedione 43 6.00 6.20 6.40 6.60 "m/z 41.00 25.54% 5000 85 100

,,,27 39 58 72 Tlfe-> 'i'' ' 'i I ' ' I ' 50 ' I ' ' ■ ' I I ' ' ' I ' ' I ■ I ■ • 60 70 80 90 100 ii6' w 6.00 6.20 6.40 6.60

25603.D NP103001.M Tue Nov 27 09:42:41 2001 Page 1

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