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GC/MS calibration results for Method 508, April 9 2002

Machine-extracted title · confidence 95%

Gas chromatography mass spectrometry calibration data for polycyclic aromatic hydrocarbons standards.

NYC-WTC_000060233–000060235

Folder label: “GCMS X 3/18/02 A 4/8/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\020409\0318REFl.D Vial: 4 Acq On 9 Apr 2002 5:58 pm Operator: McLean Sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 26 13:40:45 2002 Quant Results File: SC/^NAPR0902.R

Quant Method : C:\MSDCHEM\1...\SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan. Last Update : Fri Apr 26 13:24:19 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Compound R.T. Qlon Response Cone Unit Qvalue

34) TVnthracene 31.22 178 4094342 17.28 ug/1 100 35) Di-n-butylphthalate 33.98 149 4910455 19.96 ug/1 100 36) Fluoranthene 35.23 202 4597560 18.33 ug/1 97 39) Pyrene 35.83 202 4865939 19.38 ug/1 98 40) Buthylbenzylphthalate 38.09 149 ■1529584 16.36 ug/1 96 41) Benz(a)anthracene 39.08 228 3675486 18.85 ug/1 100 42) Chrysene 39.16 228 3823621 20.00 ug/1 99 43) Bis(2-ethylhexyl)phthalate 39.68 149 1744027 16.39 ug/1 98 45) Di-n-Octyl phthalate 41.19 149 1509485 20.75 ug/1 95 46) Benzo(b)fluoranthene 41.53 252 2540710 17.18 ug/1 95 47) Benzo(k)fluoranthene 41.59 252 3198735 18.83 ug/1 97 48) Benzo(a)pyrene 42.17 252 1702722m 13.65 ug/1 49) Indeno(1,2,3-cd)pyrene 44.35 276 686767 19.37 ug/1 98 50) Dibenz(a,h)anthracene 44.45 278 1081367 15.17 ug/1 95 51) Benzo(ghi)perylene 44.89 276 1183461 16.02 ug/1 99

(#) = qualifier out of range (m) = manual integration {+) = signals summed 0318REF1.D SCANAPR0902.M Fri Apr 26 13:47:51 2002 Page 2

NYC-WTC_000060234

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NYC-WTC_000060234Source: NYC Law Department, mirrored locally

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