GCMS data file header for sample AE00700, Jan 16 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN16\00700.D Vial: 5 Acq On : 16 Jan 2002 2:11 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 7H-Benzo[c]fluorene $$ Benz... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 36.94 0.27 ug/L 139843 Perylene-dl2 34.42 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 7H-Benzo[c]fluorene $$ Benzo[c]f... 216 C17H12 000205-12-9 27 NO 2 Butanamide, N-(2-methoxyphenyl)-... 207 C11H13NO3 000092-15-9 10 3 4-(2' , 6' ,6'-TRIMETHYL-CYCLOHEX- 1. . . 194 C13H22O 027758-30-1 10 4 Cyclopentane, 1-methyl-l-(2-meth... 138 C10H18 074764-47-9 10V*To44 Abundance Scan 2940 (36.939 min): 00700.D (-) m/z 123.10 100.00% 43 71 8 108 123 135 215 233 95 161 191 56 149 5000 173 .... ’ I’ 0 JI l'''' I ’ ’8 I ‘ ‘ ‘ l.. ‘ I >. ‘. I.... I.... I.... P ‘ I‘‘‘11‘8 rrp-i 36.60 36.80 37.00 37.20 m/z 135.10 95.87% m/z-> Abundance 40 50 60 70 80 90 100110120130140150160170180190200210220230240 #139282: 7H-Benzo[c]fluorene $$ Benzo[c]fluorene $$ 3,4-Be...

108 216 4 5000 1 * I ' ' ‘ ' I 1 ' ' ' I ' ' ’"T 36.60 36.80 37.00 37.20 95 m/z 81.10 95.69% 187 49 62 m r mm n/z-> Abundance 0 ""i""i‘ H111111 40 50 60 70 80 90 100110120130140150160170180190200210220230240 #125387: Butanamide, N-(2-methoxyphenyl)-3-oxo- 108 123 11" " r "r r'

MAAuM 207 36.60 36.'80 37'00 37'20 ' 5000 m/z 233.10 94.97% 80 149 65 92 1 134 0 — 1"1'I1'"i1'"I ""I"" I" "I" "I •189 ■ ■ ।" 1 m n/z-> 40 50 60 70 80 90 100110120130140150160170180190200210220230240 Abundance #106725: 4-(2,,6‘,6'-TRIMETHYL-CYCLOHEX-1 -EN-1 '-YL)-BUTAN... 11 r> r > ’ | ■ 81 95 123 36.60 36.80 37.00 37.20 161 m/z 43.10 93.00%

WW/MWj 107 5000 67 135 179 194

0 " " r "' r ■" 1'1" 1 ""i' ■" i' ■ i ■ ■ "I''''i’ ’’I ■"'। ""i"" 1"111"111""I |■ ■ ■■| •l H' 'l"■ > l■. iz-> 40 50 60 70 80 90 100110120130140150160 170180190200 210 220230 240 36.60 36.'80 37.00 37.20 '

)0700.D SCAN508.M Thu Jan 17 08:17:11 2002 Page 12

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