GCMS data file header for sample AE00700, Jan 16 2002

NYC 9/11 Public Portal Document

WI&p I P

Data File : C:\MSDCHEM\1\5973N\02JAN16\00700.D Vial: 5 , Acq On : 16 Jan 2002 2:11 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATARASE\WTT.EV7N **************** *** Peak Number 9 3 R.T. EstConc

36.30 2.88 u* 42

Hit# of 5 T< C+o UESTo3-OJE Qual

1 Cholestan-3-oi 3-5 95 2 5.alpha.-Cholf 3-1 95 3 Cholestan-3-or 3-6 89 4 Cholestan-3-oi 3-5 86 Abundance )0.00% 55 81

109 5000 135 213

L UM XM 255 275 1 ‘ I ' 1 36.00 36.20 36.40 36.60 0- "TI’CZATUTTTTTTTTTTTTTT m/z 231.20 91.57% n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #324507: Cholestan-3-one 231

386 5000 1 ' I I ■ ' ' I I 1 1 ' ' I ' ' 1 ' I ' ' ' ' I 95 36.00 36.20 36.40 36.60 123 163 m/z 43.10 86.12% | 0 " r " ' i " " i " ’' i1 r'' I I............... '' r ' ■' i'''' i ’" ' i'11' i'' 11111 ■ r ■ " i ■ "' r " ' r 1 ........ n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #324504: 5.alpha.-Cholestan-3-one $$ Cholestan-3-one, (5.a... 231

36.00 36.'20 3640 36.60 ' 5000 m/ z 81.05 84.31% 123 163 386 10 5 0 ‘ 111 ...................... II.... 273...................... lz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #324567: Cholestan-3-one, (5.beta.)- 43 36.00 36.20 36.40 36.60 m/z 95.10 72.40%

5000 231 386 67 95 Il 123 161 316 0 "I" "I''"I1 1.............. ........ 368 '" i " " i" " i " " i1' 11" " i" " i"111" ■' i1" 11" " i1'" i ■ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 3600 36.20 36.40 36.60

)0700.D SCAN508.M Thu Jan 17 08:17:11 2002 Page 11

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