GCMS data file header for sample AE00700, Jan 16 2002

NYC 9/11 Public Portal Document

Library Search Compound Report ■ Data File : C : \MSDCHEM\1\5973N\02JAN16\00700 . D Vial: 5 Acq On : 16 Jan 2002 2:11 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 11 3-Ethylidenecholestane Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 37.88 1.81 ug/L 949795 Perylene-dl2 34.42 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Ethylidenecholestane 398 C29H50 000000-00-0 91 2 Glaucic acid 234 C15H22O2 087745-30-0 42 3 Cyclopent[e]-1,3-oxazine, octahy... 216 C13H16N20 000000-00-0 35 4 indolo[2,1-b]quinazoline-6(12H)-... 234 C15H10N2O 113001-49-3 27 Abundance Scan 3022 (37.876 min): 00700. D (-) m/z 215.20 100.00%) 43 2 5 95

233 5000 67 121 149

................................

0 I" " P J ilb A_ ' I'' ‘ 257 383401 m/z 37.60 37.80 38.00 38.20 43.10 89.03%

_A /z-> 20 40 60 80 100120140160180200220240260 280300320 340 360 380 400 420 Abundance #331642:3-Ethylidenecholestane 81 107 135 5000: 161 37.60 37.80 38.00 38.20 243 398 m/z 95.05 77.98% O-Tp ■ ■ ■■i,T" rm । in n/z-> 20 40 60 80 100120140160180200220240260280300320340 360380400420 Abundance #165268: Glaucic acid 95 121 189 234 37.60 37.80 38.00 38.20 5000 m/z 81.10 71.38% _/

0 ।" " ।1"' p "1 i" " p'" i l"P",p"r 1 r" r1" p1111'" ’ p "1 p'" r11' p'" p " 11"'1 p ■" i" " r 1 /z—> 20 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #138739: Cyclopent[e]-1,3-oxazine, octahydro-2-(phenylimin... 2 5 37.'60 37.80 38.00 38.20 m/z 107.10 65.63%

miz-> 5000

30 65 93 135

" p *" p "11" " i1" P'''P'"P"'I 20 40 60 80 100120140160180200 220240260 280 300 320340 360380400 420 MAAMWAAn N 37.60 37.80 38.00 38.20

)0700.D SCAN508.M Thu Jan 17 08:17:11 2002 Page 13

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