GCMS data file header for sample AE00700, Jan 16 2002

NYC 9/11 Public Portal Document

Library Search Compound Report ‘ Data File : C:\MSDCHEM\1\5973N\02JAN16\00700.D Vial: 5 Acq On : 16 Jan 2002 2:11 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L *************************************************************** **** * * Peak Number 12 Palustrol $$ 4aH-Cycloprop[... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 38.38 0.46 ug/L 241229 Perylene-dl2 34.42 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Palustrol $$ 4aH-Cycloprop[e]azu... 222 C15H260 005986-49-2 25 0 2 2,3-dimethylpyrazolo[1,5-a]pyrid... 162 C9H10N2O 000000-00-0 22 3 Ledene $$ IH-Cycloprop[e]azulene... 204 C15H24 021747-46-6 22° 4 .beta.-Panasinsene 204 C15H24 000000-00-0 22 er Abundance Scan 3066 (38.378 min): 00700.D (-) m/z 55.10 100.00% 55 81 107 161 231 133 5000- 207 414

' I ' ' ' ' I ’ ' 1 i ' 1 38.00 38.20 38.40 38.60 38.80 281 oM "‘‘IT Vi I" n i " i"'11''1' i'"' ■ i " " i " " r "' i " " i" ■ ■ r 1 TTT m/z 161.10 96.39% m/z-> 40 60 80 100120140160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #148517: Palustrol $$ 4aH-Cycloprop[e]azulen-4a-ol, decahy... 1 1

5000 67 93 161 AMM,... IM A... 38.00 38.20 38.40 38.60 38.80 204 m/z 81.05 96.05% 133 I 222 0- I’ n/z-> 40 60 80 100120140160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #61947: 2,3-dimethylpyrazolo[1,5-a]pyridin-5-ol 161 38.00 38.'20 38.40 38.60 38.80 5000 95 120 m/z 107.10 91.57%

0 " i" " r. ........ p-TTT 1111111■ ‘ "11" " i" " r "11 ■ "11" " i " " i " " i " " r "' i " " i' ■" i" 1' i' n/z-> 40 60 80 100 120140160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #121623: Ledene$$ 1 H-Cycloprop{e]azulene, 1a,2,3,5,6,7,7a... 107 MAAMrye, A. 38.00 38.20 38.40 38.60 38.80 m/ z 43.10 90.50%

5000 79 161 135

189 0 I’ 11′000“ TT /z-> 40 60 80 100120140160 180 200 220 240 260 280 300 320 340 360 380 400 38.00 38.20 38.40 38.60 38.80

>0700.D SCAN508.M Thu Jan 17 08:17:12 2002 Page 14

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