GCMS reference analysis for sample AE00365, Jan-Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN15\0109R.D Vial: 2 Acq On : 15 Jan 2002 11:02 am Operator: • Sample : ref 1/9 Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 15 15:51:23 2002 Quant Results File: SCAN508.RES Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 9.72 152 995346 20.00 ug/L 0.00 10) Naphthalene-d8 13.19 136 4204775 20.00 ug/L -0.02 17) Acenaphthene-diO 18.34 164 2173090 20.00 ug/L -0.01 29) Phenanthrene-diO 22.63 188 3612706 20.00 ug/L -0.03 38) Chrysene-dl2 30.50 240 3220359 20.00 ug/L -0.01 44) Perylene-dl2 34.42 264 2239340 20.00 ug/L 0.00 System Monitoring Compounds 37) 2,4-DDD 27.73 235 289948 5.08 ug/L 0.00 Spiked Amount 5.000 Recovery = 101.60% Target Compounds Qvalue 2) n-Nitrosodimethylamine 4.00 74 114342 2.70 ug/L # 47 3) bis(2-Chloroethyl)ether 9.24 93 287687 4.18 ug/L 71 4) 1,3-Dichlorobenzene 9.61 146 201086 2.69 ug/L 99 5) 1,4-Dichlorobenzene 9.76 146 207713 2.77 ug/L 97 6) 1,2-Dichlorobenzene 10.24 146 214093 3.21 ug/L 98 7) 2,2'-oxybis (1-Chloropropa 10.68 45 415969 3.61 ug/L # 73 8) n-Nitroso-di-n-propylamine 11.06 70 200245 3.81 ug/L 73 9) Hexachloroethane 11.03 117 50743 1.89 ug/L 97 11) Nitrobenzene 11.35 77 225481 2.87 ug/L 84 12) Isophorone 12.03 82 566344 4.00 ug/L 93 13) bis(2-Chloroethoxy)methane 12.77 93 357829 4.25 ug/L 92 14) 1,2,4-Trichlorobenzene 13.11 180 176325 3.22 ug/L 96 15) Naphthalene 13.25 128 816761 4.06 ug/L 98 16) Hexachlorobutadiene 13.84 225 55764 1.91 ug/L 96 18) Hexachlorocyclopentadiene 15.96 237 7984 0.41 ug/L 94 19) 2-Chloronaphthalene 16.65 162 464406 3.87 ug/L 93 20) Dimethylphthalate 17.88 163 627332 4.37 ug/L 94 21) 2,6-Dinitrotoluene 18.06 165 63180 2.26 ug/L 81 22) Acenaphthylene 17.86 152 722211 4.13 ug/L 97 23) Acenaphthene 18.42 153 533930 4.28 ug/L 98 24) 2,4-Dinitrotoluene 19.17 165 74240 2.03 ug/L 95 25) Diethylphthalate 20.00 149 635166 4.62 ug/L 97 26) 4-Chlorophenyl-phenylether 20.03 204 282369 4.89 ug/L 83 27) Fluorene 19.91 166 620107 4.37 ug/L 97 28) Azobenzene/1,2-Diphenylhyd 20.46 77 694778 4.05 ug/L 84 30) N-nitrosodiphenylamine 20.43 169 402175 4.39 ug/L 96 31) 4-Bromophenyl-phenylether 21.44 248 160069 4.26 ug/L 88 32) Hexachlorobenzene 21.77 284 167329 4.21 ug/L 99 33) Phenanthrene 22.69 178 992469 4.99 ug/L 98 3 4) Anthracene 22.83 178 944176 4.89 ug/L 99 (#) = qualifier out of range (m) = manual integration 0109R.D SCAN508.M Tue Jan 15 15:51:23 2002 Page 1

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