GCMS reference analysis for sample AE00555, Jan-Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN29\0109R.D Vial: 2 Acq On : 29 Jan 2002 11:22 am Operator: Sample : ref 1/9 Inst : Instrumen Misc : January 29, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 30 08:26:02 2002 Quant Results File: SCAN508.RES

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508

Internal Standards R.T. Qlon Response Conc Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.72 152 1678277 20.00 ug/L 0.00 10) Naphthalene-d8 13.20 136 7070500 20.00 ug/L -0.01 17) Acenaphthene-dl0 18.34 164 3617680. 20.00 ug/L -0.01 29) Phenanthrene-d10 22.65 188 6041605 20.00 ug/L -0.02 38) Chrysene-d12 30.50 240 5463275 20.00 ug/L -0.01 44) Perylene-d12 34.42 264 4150516 20.00 ug/L 0.00

System Monitoring Compounds 37) 2,4-DDD 27.73 235 450294 4.72 ug/L 0.00 Spiked Amount 5.000 Recovery = 94.40%

Target Compounds Qvalue 2) n-Nitrosodimethylamine 4.00 74 183490 2.57 ug/L 51 3) bis(2-Chloroethyl)ether 9.24 93 465266 3.99 ug/L 71 4) 1,3-Dichlorobenzene 9.61 146 221267 1.76 ug/L 95 5) 1,4-Dichlorobenzene 9.76 146 247999 1.96 ug/L 93 6) 1,2-Dichlorobenzene 10.24 146 260920 2.32 ug/L 98 7) 2,2'-oxybis (1-Chloropropa 10.67 45 646931 3.33 ug/L # 73 8) n-Nitroso-di-n-propylamine 11.06 70 308722 3.49 ug/L 72 9) Hexachloroethane 11.03 117 37987 0.84 ug/L 98 11) Nitrobenzene 11.35 77 365956 2.77 ug/L 84 12) Isophorone 12.03 82 849235 3.57 ug/L 92 13) bis(2-Chloroethoxy)methane 12.77 93 557291 3.94 ug/L 93 14) 1,2,4-Trichlorobenzene 13.11 180 212753 2.31 ug/L 96 15) Naphthalene 13.25 128 1188022 3.51 ug/L 99 16) Hexachlorobutadiene 13.84 225 30864 0.63 ug/L 96 19) 2-Chloronaphthalene 16.65 162 682113 3.41 ug/L 93 20) Dimethylphthalate 17.88 163 940403 3.94 ug/L 95 21) 2,6-Dinitrotoluene 18.07 165 113373 2.43 ug/L 72 22) Acenaphthylene 17.86 152 1194859 4.10 ug/L 97 23) Acenaphthene 18.42 153 815045 3.93 ug/L 98 24) 2,4-Dinitrotoluene 19.19 165 142669 2.34 ug/L 81 25) Diethylphthalate 20.00 149 970424 4.24 ug/L 98 26) 4-Chlorophenyl-phenylether 20.03 204 402778 4.19 ug/L 81 27) Fluorene 19.91 166 976689 4.14 ug/L 97 28) Azobenzene/1,2-Diphenylhyd 20.46 77 1076363 3.77 ug/L 84 30) N-nitrosodiphenylamine 20.43 169 567489 3.70 ug/L 97 31) 4-Bromophenyl-phenylether 21.44 248 253762 4.04 ug/L 90 32) Hexachlorobenzene 21.78 284 233468 3.51 ug/L 94 33) Phenanthrene 22.70 178 1507799 4.53 ug/L 99 34) Anthracene 22.83 178 1448367 4.48 ug/L 99 35) Di-n-butylphthalate 24.85 149 1996261 5.12 ug/L 99 ------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration 0109R.D SCAN508.M Thu Jan 31 13:47:11 2002 Page 1

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