GCMS analysis results for sample AE00027, Jan 2002

NYC 9/11 Public Portal Document

Data File : C: \MSDCHEM\1\5973N\02JAN25\0125C40.D Vial: 2 _ Acq On : 25 Jan 2002 9:21 am Operator: Sample : cal 40 Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 28 09:00:10 2002 Quant Results File: SCAN508.RES Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 9.72 152 1368293 20.00 ug/L 0.00 10) Naphthalene-d8 13.22 136 6127406 20.00 ug/L 0.00 17) Acenaphthene-diO 18.35 164 3294985 20.00 ug/L 0.00 29) Phenanthrene-diO 22.66 188 5644346 20.00 ug/L -0.01 38) Chrysene-dl2 30.52 240 4560689 20.00 ug/L 0.01 44) Perylene-dl2 34.43 264 3342915 20.00 ug/L 0.01 System Monitoring Compounds 37) 2,4-DDD 27.58 235 42070 0.47 ug/L -0.15 Spiked Amount 5.000 Recovery = 9.40%

Target Compounds Qvalue 2) n-Nitrosodimethylamine 3.99 74 2507930 43.01 ug/L 53 3) bis(2-Chloroethyl)ether 9.28 93 3184186 36.62 ug/L 85 4) 1,3-Dichlorobenzene 9.62 146 3770185 36.72 ug/L 96 5) 1,4-Dichlorobenzene 9.77 146 3683898 35.73 ug/L 98 6) 1,2-Dichlorobenzene 10.25 146 3066701 33.50 ug/L 99 7) 2,2'-oxybis (1-Chloropropa 10.69 45 5249300 33.17 ug/L 96 8) n-Nitroso-di-n-propylamine 11.09 70 2343310 32.45 ug/L 83 9) Hexachloroethane 11.03 117 1289303 34.93 ug/L 99 11) Nitrobenzene 11.38 77 3764320 32.90 ug/L 88 12) 1sophorone 12.05 82 7429326 36.00 ug/L 94 13) bis(2-Chloroethoxy)methane 12.79 93 4734691 38.59 ug/L 94 14) 1,2,4-Trichlorobenzene 13.14 180 2755482 34.49 ug/L 98 15) Naphthalene 13.27 128 10307576 ' 35.12 ug/L 99 16) Hexachlorobutadiene 13.85 225 1331178 < 31.34 ug/L / ■ 98 18) Hexachlorocyclopentadiene 15.97 237 848740 (28.82 ug/L 97 19) 2-Chloronaphthalene 16.67 162 6132654 33.70 ug/L 95 20) Dimethylphthalate 17.93 163 7181231 33.00 ug/L 94 21) 2,6-Dinitrotoluene 18.10 165 1604652 37.81 ug/L 77 22) Acenaphthylene 17.88 152 9567665 36.06 ug/L 99 2 3) Acenaphthene 18.46 153 5748699 <30.41/ug/L 100 24) 2,4-Dinitrotoluene 19.22 165 2276386 40.96 uq/L 96 25) Diethylphthalate 20.04 149 6442058 <30.90 ug/L 98 26) 4-Chlorophenyl-phenylether 20.04 204 2678210 3056 ug/L 95 27) Fluorene 19.94 166 7395988 34.40 ug/L 99 28) Azobenzene/1,2-Diphenylhyd 20.50 77 8901063 34.24 ug/L 89 30) N-nitrosodiphenylamine 20.48 169 4541017 —3171 ug/L 98 31) 4-Bromophenyl-phenylether 21.46 248 1976283 33.65 ug/L 92 3 2) Hexachiorobenzene 21.80 284 2059771 33.19 ug/L 99 33) Phenanthrene 22.74 178 10497874 33.75 ug/L 99 3 4) Anthracene 22.86 178 10506702 34.82 ug/L 99 (#) = qualifier out of range (m) = manual integration 0125C40.D SCAN508.M Mon Jan 28 09:00:12 2002 Page 1

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