GCMS analysis results for sample AE00277, Jan 2002

NYC 9/11 Public Portal Document

Data File : C: \MSDCHEM\1\5973N\02JAN09\0109C40.D Vial: 2 Acq On : 9 Jan 2002 1:09 pm Operator: ' Sample : cal 40 Inst : Instrumen Mise : January 9, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 10 08:36:50 2002 Quant Results File: SCAN508.RES

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Wed Jan 09 12:49:14 2002 Response via : Initial Calibration DataAcq Meth : SCAN508

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.72 152 1602451 20.00 ug/L 0.00 10) Naphthalene-d8 13.20 136 7113485 20.00 ug/L -0.01 17) Acenaphthene-dlO 18.35 164 3694734 20.00 ug/L 0.00 29) Phenanthrene-diO 22.66 188 6142820 20.00 ug/L -0.01 38) Chrysene-dl2 30.51 240 5260001 20.00 ug/L 0.00 44) Perylene-dl2 34.43 264 3858746 20.00 ug/L 0.01

System Monitoring Compounds 37) 2,4-DDD 27.57 235 49034 0.50 ug/L -0.16 Spiked Amount 5.000 Recovery = 10.00%

Target Compounds Qvalue 2) N-nitroso-dimethylamine 3.98 74 2832567 41.48 ug/L 55 3) bis (2-Chloroethyl) ether 9.26 93 3832892 37.65 ug/L 77 4) 1,3-Dichlorobenzene 9.62 146 4451345 37.02 ug/L 96 5) 1,4-Dichlorobenzene 9.77 146 4389843 36.36 ug/L 98 6) 1,2-Dichlorobenzene 10.25 146 3726345 34.76 ug/L 98 7) 2,2'-oxybis (1-Chloropropa 10.68 45 6304224 34.01 ug/L 95 8) N-nitroso-di-n-propylamine 11.08 70 2701461 31.94'ug/L 83 9) Hexachloroethane 11.03 117 1526880 35.32 ug/L 99 11) Nitrobenzene 11.38 77 4333387 32.62 ug/L 85 12) Isophorone 12.04 82 8356566 34.88 ug/L 94 13) bis (2-Chloroethoxy) metha 12.79 93 5456865 38.32 ug/L 93 14) 1,2,4-Trichlorobenzene 13.12 180 3332402 35.93 ug/L 96 15) Naphthalene 13.26 128 12365509 36.29 ug/L 99 16) Hexachlorobutadiene 13.85 225 1608904 32.62 ug/L 99 18) Hexachlorocyclopentadiene 15.97 237 1293285 39.17 ug/L 97 19) 2-Chloronaphthalene 16.67 162 7129372 34.94 ug/L 93 20) Dimethylphthalate 17.92 163 8079493 33.11 ug/L 93 21) 2,6-Dinitrotoluene 18.09 165 1943126 40.83 ug/L 75 22) Acenaphthylene 17.88 152 10945932 36.79 ug/L 98 23) Acenaphthene 18.44 153 6743158 31.81/ug/L 99 24) 2,4-Dinitrotoluene 19.21 165 2712719 43.53 ug/L 91 25) Diethylphthalate 20.03 149 7492490 32.05 ug/L 99 26) 4-Chlorophenyl-phenylether 20.04 204 3219909 32.77 ug/L 91 27) Fluorene 19.93 166 8490125 35.22 ug/L 97 28) Azobenzene 20.49 77 9977062 34.22 ug/L 88 30) N-nitrosodiphenylamine 20.46 169 5470251 35.10 ug/L 98 31) 4-Bromophenyl-phenylether 21.46 248 2212138 34.61 ug/L 89 32) Hexachlorobenzene 21.79 284 2330558 34.50 ug/L 100 33) Phenanthrene 22.73 178 11913511 35.19 ug/L 100 34) Anthracene 22.85 178 12126648 36.93 ug/L 99

(#) = qualifier out of range (m) = manual integration 0109C40.D SCAN508.M Thu Jan 10 08:36:51 2002 Page 1

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