GCMS analysis results for sample AE00842, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB07\0207C40.D Vial: 2 ? Acq On : 7 Feb 2002 9:36 am Operator : Sample : cal 40 Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Feb 08 14:14:52 2002 Quant Results File: HP020702.RES

Quant Method : C:\MSDCHEM\l-..\HP020702.M (RTE Integrator) Title : 508 scan method Last Update : Fri Feb 08 10:55:14 2002 Response via : Initial Calibration DataAcq Meth : SCAN508

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.73 152 2264854 20.00 ug/L 0.00 10) Naphthalene-d8 13.22 136 10066692 20.00 ug/L 0.00 17) Acenaphthene-diO 18.35 164 5414149 20.00 ug/L 0.00 29) Phenanthrene-diO 22.67 188 9768594 20.00 ug/L 0.00 38) Chrysene-dl2 30.53 240 7826337 20.00 ug/L 0.00 44) Perylene-dl2 34.45 264 5834481 20.00 ug/L 0.00

System Monitoring Compounds 37) 2,4-DDD 27.59 235 69415 0.49 ug/L 0.00 Spiked Amount 5.000 Recovery = 9.80%

Target Compounds Qvalue 2) n-Nitrosodimethylamine 4.00 74 4141147 37.67 ug/L 100 3) bis(2-Chloroethyl)ether 9.29 93 4784037 34.12 ug/L 100 4) 1,3-Dichlorobenzene 9.63 146 5939691 35.81 ug/L 100 5) 1,4-Dichlorobenzene 9.78 146 5707087 34.78 ug/L 100 6) 1,2-Dichlorobenzene 10.26 146 4717174 33.04 ug/L 100 7) 2,2'-oxybis (1-Chloropropa 10.69 45 8242762 36.18 ug/L 100 8) n-Nitroso-di-n-propylamine 11.10 70 3936848 36.29 ug/L 100 9) Hexachloroethane 11.03 117 2147648 37.37 ug/L 100 11) Nitrobenzene 11.39 77 6369226 36.33 ug/L 100 12) Isophorone 12.06 82 12654038 37.09 ug/L 100 13) bis(2-Chloroethoxy)methane 12.80 93 7867124 35.79 ug/L 100 14) 1,2,4-Trichlorobenzene 13.14 180 4400021 34.37 ug/L 100 15) Naphthalene 13.27 128 16496629 33.73 ug/L 100 16) Hexachlorobutadiene 13.85 225 2149733 34.38 ug/L 100 18) Hexachlorocyclopentadiene 15.97 237 1679940 40.09 ug/L 100 19) 2-Chloronaphthalene 16.69 162 9817851 34.41 ug/L 100 20) Dimethylphthalate 17.94 163 12010425 36.60 ug/L 100 21) 2,6-Dinitrotoluene 18.11 165 2978957 39.34 ug/L 100 22) Acenaphthylene 17.90 152 15286645 34.88 ug/L 100 23) Acenaphthene 18.46 153 9208380 32.47 ug/L 100 24) 2,4-Dinitrotoluene 19.24 165 4297113 40.58 ug/L 100 25) Diethylphthalate 20.07 149 10063893 .33.54 ug/L 100 26) 4-Chlorophenyl-phenylether 20.05 204 4227719 3142>ug/L 100 27) Fluorene 19.95 166 12032144 34.54 ug/L 100 28) Azobenzene/1,2-Diphenylhyd 20.51 77 13903881 34,93 ug/L 100 30) N-nitrosodiphenylamine 20.49 169 6913910 (28.32 ug/L 100 31) 4-Bromophenyl-phenylether 21.47 248 3238306 33.56 ug/L 100 3 2) Hexachiorobenzene 21.81 284 3376392 33.54 ug/L 100 33) Phenanthrene 22.75 178 17475460 32.65 ug/L 100 34) Anthracene 22.87 178 17039128 31.81 ug/L 100

(#) = qualifier out of range (m) = manual integration 0207C40.D HP020702.M Fri Feb 08 14:14:52 2002 Page 1

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