GCMS reference results for sample AE00842, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB07\0111RA.D Vial : 2 Acq On : 7 Feb 2002 11:52 am Operator: Sample : ref 1/lla Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Feb 20 15:38:46 2002 Quant Results File: HP020702.RES

Quant Method : C:\MSDCHEM\l-..\HP020702.M (RTE Integrator) Title : 508 scan method Last Update : Wed Feb 20 11:48:57 2002 Response via : Initial Calibration DataAcq Meth : SCAN508

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.71 152 1439874 20.00 ug/L 0.00 10) Naphthalene-d8 13.19 136 6032743 20.00 ug/L -0.01 17) Acenaphthene-dlO 18.34 164 3184766 20.00 ug/L 0.00 29) Phenanthrene-diO 22.63 188 5357831 20.00 ug/L -0.01 38) Chrysene-dl2 30.50 240 4663164 20.00 ug/L -0.02 44) Perylene-dl2 34.42 264 3204264 20.00 ug/L -0.03

System Monitoring Compounds 37) 2,4-DDD 27.73 235 464361 5.26 ug/L 0.00 Spiked Amount 5.000 Recovery = 105.20%

Target Compounds Qvalue 2) n-Nitrosodimethylamine 4.00 74 174019 2.47 ug/L 98 3) bis(2-Chloroethyl)ether 9.24 93 434998 4.62 ug/L 99 4) 1,3-Dichlorobenzene 9.61 146 329998 3.08 ug/L 97 5) 1,4-Dichlorobenzene 9.76 146 350481 3.29 ug/L 100 6) 1,2-Dichlorobenzene 10.24 146 357873 3.77 ug/L 97 7) 2,2'-oxybis (1-Chloropropa 10.68 45 617947 4.13 ug/L 100 8) n-Nitroso-di-n-propylamine 11.06 70 282564 4.02 ug/L 94 9) Hexachloroethane 11.03 117 86485 2.35 ug/L 95 11) Nitrobenzene 11.35 77 351214 3.31 ug/L 97 12) Isophorone 12.03 82 803083 3.94 ug/L 96 13) bis(2-Chloroethoxy)methane 12.77 93 521149 3.92 ug/L 98 14) 1,2,4-Trichlorobenzene 13.11 180 270765 3.47 ug/L 94 15) Naphthalene 13.25 128 1254076 4.20 ug/L 99 16) Hexachlorobutadiene 13.84 225 84134 2.21 ug/L 97 18) Hexachlorocyclopentadiene 15.96 237 9481 0.38 ug/L 92 19) 2-Chloronaphthalene 16.65 162 710457 4.17 ug/L 96 20) Dimethylphthalate 17.88 163 944690 4.89 ug/L 96 21) 2,6-Dinitrotoluene 18.06 165 130009 2.91 ug/L 98 22) Acenaphthylene 17.86 152 1124429 4.32 ug/L 99 23) Acenaphthene 18.42 153 828785 4.82 ug/L 99 24) 2,4-Dinitrotoluene 19.17 165 160199 2.60 ug/L 90 25) Diethylphthalate 20.00 149 975890 5.43 ug/L 98 26) 4-Chlorophenyl-phenylether 20.02 204 434370 5.34 ug/L 97 27) Fluorene 19.91 166 979092 4.72 ug/L 98 28) Azobenzene/1,2-Diphenylhyd 20.46 77 1061358 4.48 ug/L 95 30) N-nitrosodiphenylamine 20.43 169 594915 4.34 ug/L 100 31) 4-Bromophenyl-phenylether 21.44 248 254266 4.70 ug/L 99 32) Hexachlorobenzene 21.77 284 263885 4.68 ug/L 99 33) Phenanthrene 22.69 178 1553683 5.19 ug/L 98 34) Anthracene 22.82 178 1459619 4.84 ug/L 98

(#) = qualifier out of range (m) = manual integration 0111RA.D HP020702.M Wed Feb 20 15:40:56 2002 Page 1

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