GCMS analysis results, Feb 25-26 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\5973N\02FEB25\0116R.D Vial: 2 . Acq On : 25 Feb 2002 12:03 pm Operator: Sample : ref 1/16 Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Feb 26 08:18:22 2002 Quant Results File: HP022102.RES Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Last Update : Mon Feb 25 10:47:59 2002 Response via : Initial Calibration DataAcq Meth : HP020702 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 9.72 152 1210905 20.00 ug/L 0.00 10) Naphthalene-d8 13.20 136 5149283 20.00 ug/L 0.00 17) Acenaphthene-diO 18.33 164 2585946 20.00 ug/L 0.00 29) Phenanthrene-diO 22.63 188 4233801 20.00 ug/L -0.01 38) Chrysene-dl2 30.49 240 3288086 20.00 ug/L -0.03 44) Perylene-dl2 34.41 264 2176407 20.00 ug/L -0.04 System Monitoring Compounds 37) 2,4-DDD 27.72 235 223362 3.96 ug/L 0.00 Spiked Amount 5.000 Recovery = 79.20% Target Compounds Qvalue 2) n-Nitrosodimethylamine 4.02 74 170508 2.87 ug/L 96 3) bis(2-Chloroethyl)ether 9.24 93 412094 5.21 ug/L 99 4) 1,3-Dichlorobenzene 9.61 146 255270 2.83 ug/L 99 5) 1,4-Dichlorobenzene 9.75 146 273471 3.05 ug/L 97 6) 1,2-Dichlorobenzene 10.24 146 273455 3.42 ug/L 97 7) 2,2'-oxybis (1-Chloropropa 10.68 45 583727 4.64 ug/L 97 8) n-Nitroso-di-n-propylamine 11.06 70 230035 3.90 ug/L 97 9) Hexachloroethane 11.04 117 53651 1.73 ug/L 94 11) Nitrobenzene 11.36 77 201407 2.22 ug/L 96 12) 1sophorone 12.04 82 703122 4.04 ug/L 97 13) bis(2-Chloroethoxy)methane 12.77 93 485647 4.28 ug/L 99 14) 1,2,4-Trichlorobenzene 13.12 180 208617 3.13 ug/L 96 15) Naphthalene 13.24 128 1090198 4.28 ug/L 98 16) Hexachlorobutadiene 13.84 225 59441 1.83 ug/L 96 19) 2-Chloronaphthalene 16.65 162 569269 4.12 ug/L 94 20) Dimethylphthalate 17.89 163 753417 4.80 ug/L 94 21) 2,6-Dinitrotoluene 18.06 165 32575 0.90 ug/L 97 22) Ac enapht hylene 17.87 152 837916 3.96 ug/L 100 2 3) Acenaphthene 18.42 153 686727 4.92 ug/L 99 24) 2,4-Dinitrotoluene 19.18 165 33714 0.67 ug/L 91 25) Diethylphthalate 19.99 149 745149 5.10 ug/L 99 26) 4-Chlorophenyl-phenylether 20.02 204 348856 5.28 ug/L 92 27) Fluorene 19.91 166 758614 4.51 ug/L 99 2 8) Azobenzene/1,2-Diphenylhyd 20.47 77 853600 4.43 ug/L 94 30) N-nitrosodiphenylamine 20.43 169 434495 4.01 ug/L 96 31) 4-Bromophenyl-phenylether 21.44 248 195019 4.56 ug/L 98 32) Hexachlorobenzene 21.76 284 207553 4.66 ug/L 95 3 3) Phenanthrene 22.69 178 1214993 5.14 ug/L 99 3 4) Anthracene 22.82 178 1085709 4.56 ug/L 99 35) Di-n-butylphthalate 24.86 149 1132177 4.14 ug/L 99 (#) = qualifier out of range (m) = manual integration 0116R.D HP022102.M Tue Feb 26 08:26:53 2002 Page 1

NYC-WTC_000003422