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GCMS reference analysis for sample AE00365, Jan-Feb 2002

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Laboratory report showing GCMS reference analysis results for sample AE00365 conducted between January 15 and 16, 2002.

NYC-WTC_000051669–000051673

Folder label: “GCMS X 1/9/02 A 1/15/02

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN15\0109R.D Vial: 2 Acq On : 15 Jan 2002 11:02 am Operator: Sample : ref 1/9 Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 15 15:51:23 2002 Quant Results File: SCAN508.RES Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508

Compound R.T. Qlon Response Cone Unit Qvalue 35) Di-n-butylphthalate 24.85 149 1238288 5.32 ug/L 99 36) Fluoranthene 26.22 202 1067014 5.43 ug/L 95 39) Pyrene 26.85 202 1135606 4.43 ug/L 95 40) Butylbenzylphthalate 29.24 149 370097 3.16 ug/L 97 41) Benzo(a)anthracene 30.44 228 881310 4.54 ug/L 99 42) Bis(2-ethylhexyl)phthalate 31.11 149 524263 3.84 ug/L 98 43) Chrysene 30.56 228 965723 5.14 ug/L 99 45) Di-n-octylphthalate 32.83 149 560527 2.67 ug/L 100 46) Benzo(b)fluoranthene 33.45 252 621315 3.50 ug/L 97 47) Benzo(k)fluoranthene 33.50 252 960100 5.66 ug/L 93 48) Benzo(a)pyrene 34.25 252 539177 3.71 ug/L 93 49) Indeno(1,2,3-cd)pyrene 37.02 276 529300 4.33 ug/L 86 50) Dibenz(a,h)anthracene 37.11 278 432131 3.95 ug/L 97 51) Benzo(g,h,i)perylene 37.72 276 501994 4.45 ug/L 92

(#) = qualifier out of range (m) = manual integration 0109R.D SCAN508.M Tue Jan 15 15:51:23 2002 Page 2

NYC-WTC_000051672

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NYC-WTC_000051672Source: NYC Law Department, mirrored locally

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