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GCMS calibration results for sample AE00365, Jan 2002

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Laboratory report showing GCMS calibration results for sample AE00365 conducted between January 15 and 16, 2002.

NYC-WTC_000051665–000051668

Folder label: “GCMS X 1/9/02 A 1/15/02

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NYC 9/11 Public Portal Document (Not Reviewed) . Data File : C:\MSDCHEM\1\5973N\02JAN15\0115C40.D Vial: 2 Acq On : 15 Jan 2002 9:22 am Operator: Sample : cal 40 Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 15 15:51:06 2002 Quant Results File: SCAN508.RES Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508

Compound R.T. Qlon Response Cone Unit Qvalue 35) Di-n-butylphthalate 24.87 149 10653364 35.44 ug/L 99 36) Fluoranthene 26.24 202 9461436 37.32 ug/L 97 39) Pyrene 26.88 202 9645226 (31.06 ug/L 98 40) Butylbenzylphthalate 29.27 149 4765339 33.52 ug/L 96 41) Benzo(a)anthracene 30.47 228 8543114 36.26 ug/L 100 42) Bis(2-ethylhexyl)phthalate 31.12 149 6247218 34.67 ug/L 97 43) Chrysene 30.59 228 6744872 29.59 ug/L 99 45) Di-n-octylphthalate 32.84 149 10345899 40.05 ug/L 100 46) Benzo(b)fluoranthene 33.48 252 7784890 35.67 ug/L 99 47) Benzo(k)fluoranthene 33.55 252 7853139 37.64 ug/L 97 48) Benzo(a)pyrene 34.28 252 7346846 41.09 ug/L 96 49) Indeno(1,2,3-cd)pyrene 37.06 276 6977826 46.47 ug/L 95 50) Dibenz(a,h)anthracene 37.14 278 5494079 40.88 ug/L 96 51) Benzo(g,h,i)perylene 37.77 276 5673145 40.86 ug/L 94

#) = qualifier out of range (m) = manual integration 115C40.D SCAN508.M Tue Jan 15 15:51:07 2002 Page 2

NYC-WTC_000051667

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NYC-WTC_000051667Source: NYC Law Department, mirrored locally

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