Laboratory report listing unknown compounds and surrogate recovery for sample AE00027 analyzed on February 7, 2002.
NYC-WTC_000050735–000050753Folder label: “GCMS X 1/4/02 A 1/25/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document i Wp/t* *MVA
Data File : C:\MSDCHEM\1\5973N\O2 JAN25\00027.D Vial: 3 . Acq On : 25 Jan 2002 4:47 pm Operator: Sample : 508 scan Inst : Insttumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ************************************************************** * * ** *** Peak Number 8 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.89 3.52 ug/L 1502490 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H1404 015745-87-6 33 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 3 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 4 Silane, tetramethyl- (CAS) $$ Te... 88 C4H12Si 000075-76-3 9 Abundance Scan 220 (5.885 min): 00027.D (-) m/z 73.10 100.00% 73
5000 43 —————1——TTTTTTT 87 5.60 5.80 6.00 6.20 ....................... , 55 . bi 103 rpe.... 'A'. rep‘ i' u ■ r ■ " i'1'11'1111 ’’’ I' ■ ■' i1 ■'' i'' " i'''' i' m/z 43.10 23.57% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73
5000 —u9——TTTTTTT 5.60 5.80 6.00 6.20 43 m/z 45.10 9.58% 27 55 87 TTTTTTTTTTTTT+rTTTTr II " " I H " 113 174 i' "' r " ' i" " r ' " i'" 11'1 “ i" " i' 1 ' I ' _ miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 *i"T‘" 1 ' 5.60 5.80 6.00 6.20 5000 m/ z 41.10 8.86% __ 43 27 87 55 TTTTTTTTTTTTT TTTTTTTTTT TTpr "1111 h i h 113 ।"11"1111 u 11" " । 174 ।।। ’ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... 1 1 i ' b 30 5.60 5.80 6.00 6.20 73 m/z 71.10 6.80%
5000 44 58
15 Tryre 11 4 ml Irn i ■' HI'1" I'' i" " r " ' i1"11H ° iH " i" " i'"11111' I" " i' TTIUPTTTTTTT /z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20
20027.D SCAN508.M Mon Jan 28 09:49:30 2002 Page 10
NYC-WTC_000050748
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NYC-WTC_000050754
Laboratory report listing unknown compounds and surrogate recovery for sample AE00108 analyzed on February 7, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051586
Laboratory report showing GCMS analysis results for sample AE00613 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050683
Laboratory report listing unknown compounds and surrogate recovery for sample AE00166 analyzed on February 13, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050519
Laboratory report for sample AE00169 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051930
GCMS analysis log for sample AE00737 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052251
Laboratory report showing GCMS analysis of sample AE00842 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051967
GCMS analysis log for sample AE00739 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050481
Laboratory report for sample AE00167 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051549
Laboratory report showing GCMS analysis results for sample AE00556 conducted on February 1, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050645
Laboratory report listing unknown compounds and surrogate recovery for sample AE00110 analyzed on February 13, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050539
Laboratory report for sample AE00247 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000006085
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03245 conducted on March 15, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000050702
Administrative record from DEP Box 28 documenting CCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050703
Technical log recording method parameters and sample processing details for a DEP laboratory procedure between January 4 and 25, 2002.
Filed in the same folder
NYC-WTC_000050705
Laboratory report listing concentrations of volatile organic compounds in sample AE00027 analyzed on January 25, 2002.
Filed in the same folder
NYC-WTC_000050709
Reference standard GCMS analysis for sample AE00027 performed on January 25, 2002, providing quality control results.
Filed in the same folder
NYC-WTC_000050716
Laboratory report showing non-detect results for volatile organic compounds in a GCMS blank analyzed on January 25-February 7, 2002.
Filed in the same folder