Laboratory report listing unknown compounds and surrogate recovery for sample AE00027 analyzed on February 7, 2002.
NYC-WTC_000050735–000050753Folder label: “GCMS X 1/4/02 A 1/25/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document J
Data File : C: \MSDCHEM\1\5973N\02JAN25\00027.D Vial: 3 . Acq On : 25 Jan 2002 4:47 pm Operator: Sample : 508 scan Inst : InstrUmen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 3-Buten-2-ol, 2-methyl- Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 5.01 0.09 ug/L 36614 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual l 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 45 2 Trifluoroacetic acid, 2-tetrahyd... 198 C7H9F3O3 000000-00-0 33 3 Butane, 2-bromo-2-methyl- $$ ter... 150 C5HllBr 000507-36-8 28 4 2,4,6-Trimethyl-l-nonene 168 C12H24 055771-40-9 12 Abundance Scan 143 (5.006 min): 00027. D (-) m/z 43.10 100.00% 43 71
5000’ 55 ........ 84.............................................. AWNA 1WA4AA.,.. 4.60 4.80 5.00 5.20 5.40 49 J - m/z 71.10 95.08% /z-> 10 20 30 40 50 60 70I 80 90 100 110 120 130 Abundance #4085:3-Buten-2-ol, 2-methyl- 43 7
5000 -A- ‘18* 59 4.60 4.80 5.00 5.20 5.40 27 m/ Z 41.10 66.40% 53
m/z-> 1 ' I 1 ' ' 1 I 1 1 ■ ■ I ' 1 ■ ■ i ' 10 20 30 40 50 +,. — 44 60 70I 86 BTII1—9—m—TTPTTT 80 90 100 110 120 130 1 Abundance #111395: Trifluoroacetic acid, 2-tetrahydrofurylmethyl ester 43 71
4.60 TIT 4.80 SAMeepA. 5.00 5.20 5.40 5000 m/z 69.10 34.95% 31 51 37 ||, | 57 1 1 1 1 n. '. T-p- — 1 11/195................... m/z-> 10 20 30 40 50 60 70I 80 90 100 110 120 130 Abundance #45652: Butane, 2-bromo-2-methyl- $$ tert-Amyl bromide $$... • i 1 ■ ■ ■ i 1 ' 43 71 4.60 4.80 5.00 5.20 5.40 m/Z 55.00 31.32% 5000’ 27 55
15 TT-p-rS-r-j-r —34 , , , , 1...........1......................................... 121 A...... -r-pn-r-r-pr Mr.A-ru ,r /z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 4.60 4.80 5.00 5.20 5.40
00027.D SCAN508.M Mon Jan 28 09:49:30 2002 Paige 9
NYC-WTC_000050747
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NYC-WTC_000050754
Laboratory report listing unknown compounds and surrogate recovery for sample AE00108 analyzed on February 7, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051586
Laboratory report showing GCMS analysis results for sample AE00613 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050683
Laboratory report listing unknown compounds and surrogate recovery for sample AE00166 analyzed on February 13, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050519
Laboratory report for sample AE00169 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051930
GCMS analysis log for sample AE00737 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052251
Laboratory report showing GCMS analysis of sample AE00842 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051967
GCMS analysis log for sample AE00739 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050481
Laboratory report for sample AE00167 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051549
Laboratory report showing GCMS analysis results for sample AE00556 conducted on February 1, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050645
Laboratory report listing unknown compounds and surrogate recovery for sample AE00110 analyzed on February 13, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050539
Laboratory report for sample AE00247 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000006085
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03245 conducted on March 15, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000050702
Administrative record from DEP Box 28 documenting CCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050703
Technical log recording method parameters and sample processing details for a DEP laboratory procedure between January 4 and 25, 2002.
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NYC-WTC_000050705
Laboratory report listing concentrations of volatile organic compounds in sample AE00027 analyzed on January 25, 2002.
Filed in the same folder
NYC-WTC_000050709
Reference standard GCMS analysis for sample AE00027 performed on January 25, 2002, providing quality control results.
Filed in the same folder
NYC-WTC_000050716
Laboratory report showing non-detect results for volatile organic compounds in a GCMS blank analyzed on January 25-February 7, 2002.
Filed in the same folder