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GCMS analysis results for sample AE00555, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis results for sample AE00555 conducted on February 1, 2002.

NYC-WTC_000051531–000051548

Folder label: “GCMS X 1/9/02 A 1/29/02

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Scanned page image, NYC-WTC_000051540
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

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Data File : C:\MSDCHEM\1\5973N\02JAN29\00555.D Vial: 1 • Acq On : 29 Jan 2002 2:32 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 Butanoic acid, 2-methyl-, m.. Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 4.62 0.06 ug/L 31041 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Butanoic acid, 2-methyl-, methyl... 116 C6H12O2 000868-57-5 43 2 2-Buten-l-ol, 3-methyl- (CAS) $$... 86 C5H10O 000556-82-1 38 3 2-Buten-l-ol, 3-methyl- (CAS) $$... 86 C5H10O 000556-82-1 38 4 2-Buten-l-ol, 2-methyl- (CAS) $$... 86 C5H10O 004675-87-0 38 Abundance Scan 109 (4.618 min): 00555.D (-) m/ z 88.00 100.00% 83 57 71 41

5000 101 MAAAAALLWAAAA— ■n/z-> • • I •«I • I ’ ‘»'1 • ’ I • I HP) 51

20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 I " '' I * TT L TT-p-i-i-rp- 4 20 m/z 4.40 71.10 4.60 4.80 5.00 81.99% Abundance #16441: Butanoic acid, 2-methyl-, methyl ester (CAS) $$ Me... 88 ft 57

5000 ... . ' 'I । N < — 41 4.20 4.40 4.60 4.80 5.00 29 101 m/z 57.10 77.17%

iz-> 1 'I""I" 1 m TT + I ""I""I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 69 tT '" r ' “ r

Abundance #4075: 2-Buten-1-ol, 3-methyl- (CAS) $$ Prenol $$ 2-METHYL... 71 41 4.20 4.40 4.60 4.80 5.00 5000 m/z 41.10 72.81% 53 86

m/z-> " r "' i" " r " ■ i' " ■ i II,.... ,..... 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 ' r " ' i" " r " ‘ i " " r

Abundance #4072: 2-Buten-1-ol, 3-methyl- (CAS) $$ Prenol $$ 2-METHYL... 7h 4.20 4.40 4.60 4.80 5.00 m/z 43.10 59.07%

5000 27 39 53

m/z-> " r111 r " i1 ’" r " 59 TIITTTT tmmmm 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 66 | 86 _/MAAAAAaA/ 420 4.40 4.60 4.80 5.00

10555.D SCAN508.M Wed Jan 30 09:01:52 2002 Page 6

NYC-WTC_000051540

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NYC-WTC_000051540Source: NYC Law Department, mirrored locally

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