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GCMS analysis results for sample AE00027, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report listing unknown compounds and surrogate recovery for sample AE00027 analyzed on February 7, 2002.

NYC-WTC_000050735–000050753

Folder label: “GCMS X 1/4/02 A 1/25/02

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Scanned page image, NYC-WTC_000050749
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN25\00027.D Vial: 3 . Acq On : 25 Jan 2002 4:47 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 2-Propanol, l,l'-oxybis- (C... Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 9.55 0.09 ug/L 39007 1,4-Diehlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# " Qual 1 2-Propanol, l,l'-oxybis- (CAS) $... 134 C6H1403 000110-98*5 39 2 2-Propanol, l,l'-oxybis- (CAS) $... 134 C6H1403 000110-98-5 39 3 2,3-Epoxy-3-methyl-6-methoxyheptane 158 C9H18O2 088083-53-8 9 4 MIXTURE OF: 5,6-DIHYDRO-6-METHYL... 112 C6H802 000108-54-3 9 Abundance Scan 541 (9.550 min): 00027.D (-) m/z 59.10 100.00% 59 45 5000 103 73 86

m/z-> 20 ■ ।1 >1 ■I■।'।■।■.। 30 ।11 .. Il, #‘bVvt"h‘stdn**vsdt<*‘v**2k**‘If 40 50 60 70 80 90 100 110 120 130 140 150 160 9.20 m/z 9.40 45.10 9.60 9:80 55.24% Abundance #29205:2-Propanol, 1,1‘-oxybis- (CAS) $$ Dipropylene glyc... 59 31 5000 45 9.20 9.40 9.60 9.80 103 m/z 103.10 41.99%

m/z- > 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #29204:2-Propanol, 1,1 ‘-oxybis- (CAS) $$ Dipropylene glyc... 59 9.20 9.40 9.60 9.80 5000 31 45 m/Z 73.10 31.80% 103

r T 460 ' 1111 ‘ I " b' i1 >I*••‘। 1 m/z-> 20 30 40 50 70 80 90 100 110 120 130 140 150 160 Abundance #57909:2,3-Epoxy-3-methyl-6-methoxyheptane 59 9.20 9.40 9.60 9.80 m/z 41.10 29.98% 45 5000' 72

.. „.MM,Om 30 99 86 TIt 1 I, •111 * 126 143 158 1 r ■ ■11 ■ ■' ■ i' ■ • ■ i ■ 1 H i1''111''1111 ■' i1 r m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 9.20 9.40 9.60 9.80

30027.D SCAN508.M Mon Jan 28 09:49:30 2002 Page 11

NYC-WTC_000050749

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NYC-WTC_000050749Source: NYC Law Department, mirrored locally

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