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GCMS analysis results for sample AE00027, Feb 2002

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Laboratory report listing unknown compounds and surrogate recovery for sample AE00027 analyzed on February 7, 2002.

NYC-WTC_000050735–000050753

Folder label: “GCMS X 1/4/02 A 1/25/02

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NYC 9/11 Public Portal Document X P*** L‘

Data File : C:\MSDCHEM\1\5973N\02JAN25\00027.D Vial: 3 • Acq On : 25 Jan 2002 4:47 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method . Library : C:\DATABASE\WILEY7N.L ******************************************************************** * Peak Number 10 2-Propanol, 1- (2-methoxypro. . . Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 9.85 0.15 ug/L 63539 1,4-Diehlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1-(2-methoxypropoxy)... 148 C7H16O3 013429-07-7 83 2 Butanoic acid, 2-hydroxy- $$ But... 104 C4H803 000565-70-8 9 3 TRIPROPYLENE GLYCOL 2 192 C9H20O4 000000-00-0 9 4 Butane, 2-methoxy- $$ Ether, sec.. 88 C5H120 006795-87-5 9 Abundance Scan 567 (9.847 min): 00027.D (-) m/z 59.10 100.00% 50

5000

45 - .......... I 73 86 104 r ' M i111111 TTTTmuuumuuDT M. m/z. 9.60 9.80 45.10 —AAA 10.00 10.20 15.37% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #43942:2-Propanol, 1-(2-methoxypropoxy)-$$ 1-(2-Methoxyp... 50

5000 Trnmm—memTTTTTuur 9.60 9.80 10.00 10.20 m/z73.10 12.75% 31 45 - 73........... 104........ 130................. TTTTT.MTT I । । i i । i'l i . PVUTPoupi । । IT । n । , , , , । , UTT /z- > 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #10063: Butanoic acid, 2-hydroxy- $$ Butyric acid, 2-hydro... 50 31 AMNAA9.60 9.80 TTT 10.00 10.20 5000 m/z 43.10 12.09% N 45 A n/z-> 20 111'1'I1 30 40 1i1' 50 60 .. I., 76 104 111oosss141p****n****]II**1***G*V**II 70 80 90 100 110 120 130 140 150 160 Abundance #102327: TRIPROPYLENE GLYCOL 2 59 9.60 9.80 10.00 10.20 m/ z 41.10 9.75%

5000

m/z—> 45 ----- 20 30 40 50 60 70 —9 80 103 117 130 90 100 110 120 130 140 150 160 161 -MAA 9.60 9.80 10.00 10.20

30027.D SCAN508.M Mon Jan 28 09:49:30 2002 Page 12

NYC-WTC_000050750

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NYC-WTC_000050750Source: NYC Law Department, mirrored locally

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