GCMS reference analysis results for sample AE07311, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR1302\1965.D Vial: 3 Acq On : 13 Mar 2002 12:01 pm Operator: Sample : re-extraction Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L

Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.20 0.37 ug/1 45490 1,4-Dichlorobenzene-d4 12.31

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 33 2 Formamide/ N,N-dimethyl- 73 C3H7NO 000068-12-2 5 3 N-Ethyl formamide 73 C3H7NO 000627-45-2 5 4 1,3-Dioxolane 74 C3H602 000646-06-0 4 Abundance Scan 343 (8.196 min): 1965.D (-j m/z 73.0,0 100.00% 73

5000 43 / \ 1

111151 57..... . 1 Bon r1 1 87'''........... 103 ■ 7.80. 8.00 8.20 8.40 8.60 ' ' i ' ’ 1 ■ i ' 1 ' 1 i ' ’ ' r I 1 1 ' ' I ' ' 1 ' . ........ m/z 43.05 1 1 1 1 ' ) 1 29.22% m/z-> 10 20 30 40 50 60 70 80 !90 100 110 | Abundance #63573: 3-Pentanol, 3-methyl- 73 5000- 7.80 8.00 8.20 8.40 8.60 55 m/z 44.95 11.72% 27 45 87 ■ ' । li 1 । ■ ■ 1 39, , ' . .... . i 1 ' > ■ i > ■ ■ ■ i ■ ■ ■ ■ l ■ r > ■ । 1 ■ > । I > 1 1 । I ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance i ■ .

44 73 ■ 1 । 1 r 1 ■ । 1 r 7.80 8.00__ 8.20 8.40 8.60 | 5000 m/z 41.05 9.73% 30 15 39 58 ' 1 ' I ' ' ' ' I ' ' r--II ' ' I m/z-> Abundance 10 20 30 40 50 60 70 i#292: N-Ethylformamide 80 90 100 110 .......... .A..... .. 33 7.80 8.00 8.20__ 8.40 8.60 73 m/z 71.00 7.54% 5000 44 58

.35. -_ _ 2 1 ' ' 1 1 1 1 ' I ' 1 1 1 1 ' ' 1 L 'I I I ' I I I 1 I I I 1 1 I 1 I I I I I I I I I I I I I I I I I 11 I ■ ■ । ■ ■ ■ ■ । ■ m/z-> 10 20 30 __ 40___ 50 60 70 80____ 90 100 110_ 7.80 8.00 8.20 8.40 8.60

1965.D GCMS0208.M Wed Mar 27 11:56:40 2002 Page 1

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