Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10199 on May 10, 2002.
NYC-WTC_000044926–000044941Folder label: “GCMS X 4/30/02 A 5/8/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\MSDCHEM\1\DATA\050802\10199.D Vial: 17 Acq On 9 May 2002 4:27 am Operator: Mclean Sample 4/30 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L
Peak Number 4 Thiocyanic acid, 2-benzothi... Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T.
22.58 0.30 ug/L 365604 Phenanthranene- dl 0 22.95 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-050 2 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 45 3 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 42 4 4-Hydroxy-3,5-dimethylcinnamic acid 192 C11H1203 1000132-15-8 38 Abundance Scan 3319 (22.580 min): 10199.D (-3312) (-) m/z 192.10 100.00% 192
5000
I | I T-1 I J r i I i l I I I ] | 11 1] I
22.20 22.40 22.60 22.80 23.00
m/z-> 42 52 66 82 96 118 132 | 160 0 I | I ■ > I | r > ■ < | I I > I '| I I 'I I | I T I I | I I I I I i I > | > I I I | I I I I | I > I / | / > < I' | ' I ! I > | I I ' I '! | ।| > > . ! | I T I I | ! I I I | 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 U m/z 191.10 19.54% Abundance #80870: Thiocyanic acid, 2-benzothiazolyl ester 192
5000 22.20 22.40 22.60 22.80 23.00 m/z 146.10 15.53% 45 I 7 , , T , 198 122 134 148 160 o ........................... I I I I I I I I I I I I ii........... I I I I I i । । । । । | i । ! । । I । । i । । । I i । । । । I’। । । i । । I 1 । i [ । I। । । । riH | । । । । | i i'l । । । । । । । । r । । |r I I > TT-J-r m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80953: 2-Propenal, 3-(3,4-dimethoxyphenyl)- 192 161 00 — 22.20 22.40 22.60 22.80 23.00 5000 m/ z 193.10 13.19% 77 121 149 177 91 103 138 52 64 1 m/z-> 0 .................................... ii.......... |......... .......... i | I > i r | i t i i | > i i I | I I i । | । I Ti | I I I I | I I I
20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 4-J ।.. I... Il....ll , ........ 4 I I I I I I I I I I I I I I I I I I I I I II I I I r II I I I I I I
Abundance #81033: Phenanthrene, 9-methyl- TIT 192 22.20 22.40 22.60 22.80 23.00 m/ z 96.00 10.53%
5000
96
m/z-> 0T I 29 39 51 63 75 83
20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 j ' I 'I I I I I pi 'I I I [ I11 I I rtn i'll i" I 111 I I I 115 126 139 152 ~| i r i i । i i । » । । i i r । i i i i 165 I 176 *i । i । । r i p ' r 1111 4— ................... I|।I 1 i | * I
22.20 22.40 22.60 22.80 23.00 I i I ............. i I ! |—| । I )1 ) 1
10199.D 050102.M Thu May 09 13:36:02 2002 Page 7
NYC-WTC_000044937
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000044994
Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10204 on May 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045075
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE10303 conducted on May 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044885
Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10198 on May 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043938
Gas chromatography-mass spectrometry analysis report for sample AE09968, detecting unknown compounds and 2,4-DDD surrogate with 78% recovery, dated May 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045171
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE10308 conducted on May 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045155
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE10307 conducted on May 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044942
Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10200 on May 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044978
Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10203 on May 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045137
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE10306 conducted on May 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024153
Document noting low recovery in GCMS scan of sample AE10205 and subsequent re-extraction yielding 85% recovery.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022886
GCMS analytical report for environmental sample AE09332 including surrogate compound data from May 15, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025447
Laboratory report showing GCMS results for sample AE11421 analyzed on May 30, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000044856
Department of Environmental Protection GCMS analysis record for the World Trade Center site dated April-May 2002.
Filed in the same folder
NYC-WTC_000044857
Administrative page listing laboratory method details, sample volumes, and surrogate addition parameters for environmental testing on April 30, 2002.
Filed in the same folder
NYC-WTC_000044858
Laboratory report showing blank sample analysis results for volatile organic compounds using gas chromatography-mass spectrometry on May 9, 2002.
Filed in the same folder
NYC-WTC_000044873
Laboratory report showing gas chromatography-mass spectrometry calibration results for volatile organic compounds in sample AE10198 on May 9, 2002.
Filed in the same folder
NYC-WTC_000044877
Laboratory report showing gas chromatography-mass spectrometry reference standard results for volatile organic compounds in sample AE10198 on May 9, 2002.
Filed in the same folder